4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenylsulfur trifluoride

Base Information

Chemical Name:4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenylsulfur trifluoride
CAS No.:1259293-84-9
Molecular Formula:C₁₆H₁₉F₉O₂S
Molecular Weight:446.377
Hs Code.:

Synonyms:4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenylsulfur trifluoride

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Chemical Property of 4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenylsulfur trifluoride

Chemical Property:

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Technology Process of 4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenylsulfur trifluoride

There total 5 articles about 4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenylsulfur trifluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1259293-82-7
bis[4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenyl] disulfide

: 1259293-84-9
4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenylsulfur trifluoride

Guidance literature:: bis[4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenyl] disulfide; With chlorine; cesium fluoride; In acetonitrile; at 20 ℃;

In acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ja106343h

Reference yield:

: 1006064-11-4
bis[4-tert-butyl-2,6-bis(methoxymethyl)phenyl] disulfide

: 1259293-84-9
4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenylsulfur trifluoride

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogen bromide; acetic acid / 4 h / 65 °C

2.1: sodium / 70 °C / Inert atmosphere

2.2: 24 h / 110 °C / Inert atmosphere

3.1: chlorine; cesium fluoride / acetonitrile / 20 °C

3.2: 2 h / 20 °C / Inert atmosphere

With hydrogen bromide; sodium; chlorine; acetic acid; cesium fluoride; In acetonitrile;
DOI:10.1021/ja106343h

Reference yield:

: 1259294-21-7
bis[2,6-bis(bromomethyl)-4-tert-butylphenyl] disulfide

: 1259293-84-9
4-tert-butyl-2,6-bis(2,2,2-trifluoroethoxymethyl)phenylsulfur trifluoride

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium / 70 °C / Inert atmosphere

1.2: 24 h / 110 °C / Inert atmosphere

2.1: chlorine; cesium fluoride / acetonitrile / 20 °C

2.2: 2 h / 20 °C / Inert atmosphere

With sodium; chlorine; cesium fluoride; In acetonitrile;
DOI:10.1021/ja106343h