N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylleucine methyl ester

Base Information

Chemical Name:N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylleucine methyl ester
CAS No.:395647-21-9
Molecular Formula:C₂₇H₃₆N₄O₅
Molecular Weight:496.607
Hs Code.:

Synonyms:N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylleucine methyl ester

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Chemical Property of N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylleucine methyl ester

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Technology Process of N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylleucine methyl ester

There total 4 articles about N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylleucine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 395647-14-0
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}leucine methyl ester

: 395647-21-9
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylleucine methyl ester

Guidance literature:: With dmap; In acetonitrile;
DOI:10.1016/S0040-4039(01)01350-8

Reference yield:

: 20691-84-3
m-methyl red

: 395647-21-9
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylleucine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / DCC; HOBt / dimethylformamide

2: 99 percent / DMAP / acetonitrile / 20 °C

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b212470j

Reference yield:

: 7517-19-3
methyl (L)-leucinate hydrochloride

: 395647-21-9
N-{3-[(N,N-dimethylaminophenyl)-4'-diazenyl]benzoyl}-N-tert-butyloxycarbonylleucine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / DCC; HOBt / dimethylformamide

2: 99 percent / DMAP / acetonitrile / 20 °C

With dmap; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In N,N-dimethyl-formamide; acetonitrile;
DOI:10.1039/b212470j