(CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br

Base Information

• Chemical Name: (CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br
• CAS No.: 1237133-01-5
• Molecular Formula: Br*C₄₅H₇₂NO₂
• Molecular Weight: 738.976
• Mol file: 1237133-01-5.mol

Synonyms:(CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br

Chemical Property of (CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br

There total 5 articles about (CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3⁽¹⁺⁾*Br^(1-)=(CH₂CHCH₂)3CC₆H₄OC₄H₈OCH₂C₆H₄N(C₆H₁₃)3Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

tri-n-hexylamine (102-86-3) + C27H33BrO2 (1209005-73-1) → (CH2CHCH2)3CC6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=(CH2CHCH2)3CC6H4OC4H8OCH2C6H4N(C6H13)3Br (1237133-01-5)

Guidance literature:

In acetonitrile; at 80 ℃; for 16h;

DOI:10.1002/ejic.200901141

Reference yield:

C11H15IO2 (1237132-95-4) → (CH2CHCH2)3CC6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=(CH2CHCH2)3CC6H4OC4H8OCH2C6H4N(C6H13)3Br (1237133-01-5)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C

2: phosphorus tribromide / toluene / 4 h / 20 °C

3: acetonitrile / 16 h / 80 °C

With phosphorus tribromide; potassium carbonate; In N,N-dimethyl-formamide; toluene; acetonitrile;

DOI:10.1002/ejic.200901141

Reference yield:

C27H34O3 (1209005-72-0) → (CH2CHCH2)3CC6H4OC4H8OCH2C6H4N(C6H13)3(1+)*Br(1-)=(CH2CHCH2)3CC6H4OC4H8OCH2C6H4N(C6H13)3Br (1237133-01-5)

Guidance literature:

Multi-step reaction with 2 steps

1: phosphorus tribromide / toluene / 4 h / 20 °C

2: acetonitrile / 16 h / 80 °C

With phosphorus tribromide; In toluene; acetonitrile;

DOI:10.1002/ejic.200901141

upstream raw materials:

C₂₇H₃₄O₃

tri-n-hexylamine

C₂₇H₃₃BrO₂

[4-(4-chlorobutoxy)phenyl]methanol