4-((1-tert-butyl)-1H-imidazolium-3-yl)methyl-1-(2,6-diisopropylphenyl)-3-methyl-1H-1,2,3-triazol-3-ium bromide trifluoromethanesulfonate

Base Information

Chemical Name:4-((1-tert-butyl)-1H-imidazolium-3-yl)methyl-1-(2,6-diisopropylphenyl)-3-methyl-1H-1,2,3-triazol-3-ium bromide trifluoromethanesulfonate
CAS No.:1392271-00-9
Molecular Formula:Br*CF₃O₃S*C₂₃H₃₅N₅
Molecular Weight:610.539
Hs Code.:

Synonyms:4-((1-tert-butyl)-1H-imidazolium-3-yl)methyl-1-(2,6-diisopropylphenyl)-3-methyl-1H-1,2,3-triazol-3-ium bromide trifluoromethanesulfonate

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Chemical Property of 4-((1-tert-butyl)-1H-imidazolium-3-yl)methyl-1-(2,6-diisopropylphenyl)-3-methyl-1H-1,2,3-triazol-3-ium bromide trifluoromethanesulfonate

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Technology Process of 4-((1-tert-butyl)-1H-imidazolium-3-yl)methyl-1-(2,6-diisopropylphenyl)-3-methyl-1H-1,2,3-triazol-3-ium bromide trifluoromethanesulfonate

There total 4 articles about 4-((1-tert-butyl)-1H-imidazolium-3-yl)methyl-1-(2,6-diisopropylphenyl)-3-methyl-1H-1,2,3-triazol-3-ium bromide trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1392270-94-8
1-(tert-butyl)-3-((1-(2,6-diisopropylphenyl)-1H-1,2,3-triazol-4-yl)methyl)-1H-imidazolium bromide

: 333-27-7
methyl trifluoromethanesulfonate

: 1392271-00-9
4-((1-tert-butyl)-1H-imidazolium-3-yl)methyl-1-(2,6-diisopropylphenyl)-3-methyl-1H-1,2,3-triazol-3-ium bromide trifluoromethanesulfonate

Guidance literature:: In dichloromethane; at -78 - 20 ℃; regioselective reaction; Inert atmosphere;
DOI:10.1021/om3004543

Reference yield:

: 1392270-89-1
1-(tert-butyl)-3-prop-2-yn-1-yl-1H-imidazolium bromide

: 1392271-00-9
4-((1-tert-butyl)-1H-imidazolium-3-yl)methyl-1-(2,6-diisopropylphenyl)-3-methyl-1H-1,2,3-triazol-3-ium bromide trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide; triethylamine / methanol; water / 20 °C

2: dichloromethane / -78 - 20 °C / Inert atmosphere

With copper(l) iodide; triethylamine; In methanol; dichloromethane; water;
DOI:10.1021/om3004543

Reference yield:

: 45676-04-8
1-tert-butylimidazole

: 1392271-00-9
4-((1-tert-butyl)-1H-imidazolium-3-yl)methyl-1-(2,6-diisopropylphenyl)-3-methyl-1H-1,2,3-triazol-3-ium bromide trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1,4-dioxane; acetonitrile / 24 h / Reflux

2: copper(l) iodide; triethylamine / methanol; water / 20 °C

3: dichloromethane / -78 - 20 °C / Inert atmosphere

With copper(l) iodide; triethylamine; In 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;
DOI:10.1021/om3004543