sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate

Base Information

Chemical Name:sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate
CAS No.:1428128-01-1
Molecular Formula:C₂₃H₁₇ClF₂NO₃*Na
Molecular Weight:451.832
Hs Code.:

Synonyms:sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate

Suppliers and Price of sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate

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Technology Process of sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate

There total 6 articles about sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1428130-14-6
methyl 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate

: 1428128-01-1
sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate

Guidance literature:: With sodium hydroxide; In ethanol; water; at 80 ℃;

Reference yield:

: 632625-91-3
1-(bromomethyl)-2,4-difluorobenzene

: 1428128-01-1
sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1: sodium tetrahydroborate / ethanol / 0 °C

2: phosphorus tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere

3: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

4: sodium hydroxide / ethanol; water / 80 °C

With sodium tetrahydroborate; phosphorus tribromide; potassium carbonate; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 23915-07-3
1-(bromomethyl)-2,4-difluorobenzene

: 1428128-01-1
sodium 1-(5-chloro-2-((2,4-difluorobenzyl)oxy)benzyl)indoline-4-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / N,N-dimethyl-formamide / 40 °C

2: sodium tetrahydroborate / ethanol / 0 °C

3: phosphorus tribromide / dichloromethane / 0 - 20 °C / Inert atmosphere

4: potassium carbonate / N,N-dimethyl-formamide / 0 - 20 °C

5: sodium hydroxide / ethanol; water / 80 °C

With sodium tetrahydroborate; phosphorus tribromide; potassium carbonate; sodium hydroxide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;