1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde

Base Information

Chemical Name:1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde
CAS No.:155091-94-4
Molecular Formula:C₄₁H₃₆N₆O
Molecular Weight:628.776
Hs Code.:

Synonyms:1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde

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Chemical Property of 1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde

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Technology Process of 1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde

There total 21 articles about 1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 155091-95-5
5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole

: 155091-94-4
1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde

Guidance literature:: 5-butyl-2-hydroxymethyl-1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>imidazole; With oxalyl dichloride; In dichloromethane; dimethyl sulfoxide; at -78 ℃;

With triethylamine; In dichloromethane; at -60 - 20 ℃; for 1h;
DOI:10.1016/j.ejmech.2012.07.040

Reference yield:

: 146953-86-8
4-n-Butyl-imidazole

: 155091-94-4
1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde

Guidance literature:: Multi-step reaction with 6 steps

1: 84 percent / Et₃N / acetonitrile / 1 h / Ambient temperature

2: 38 percent / acetonitrile / 1.) reflux, 4 h; 2.) RT

3: 37 percent / H₂O / 6 h / 140 °C / Curtius tube

4: 98 percent / Na/NH₃(l) / methanol / 0.08 h

5: 85 percent / MnO₂ / CH₂Cl₂ / Ambient temperature

6: cesium carbonate / dimethylformamide / Ambient temperature

With manganese(IV) oxide; ammonia; sodium; caesium carbonate; triethylamine; In methanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 148674-47-9
4-butyl-1H-imidazole-2-carboxaldehyde

: 133051-88-4
N-(triphenylmethyl)-5-<4'-(bromomethyl)biphenyl-2-yl>tetrazole

: 155092-07-2
1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-4-butylimidazole-2-carboxaldehyde

: 155091-94-4
1-<<2'-<(N-triphenylmethyl)tetrazol-5-yl>biphenyl-4-yl>methyl>-5-butylimidazole-2-carboxaldehyde

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 18h; regioselective reaction; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.07.040