2,2-diphenylcyclobutanecarboxylic acid

Base Information

Chemical Name:2,2-diphenylcyclobutanecarboxylic acid
CAS No.:286850-82-6
Molecular Formula:C₁₇H₁₆O₂
Molecular Weight:252.313
Hs Code.:

Synonyms:2,2-diphenylcyclobutanecarboxylic acid

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Chemical Property of 2,2-diphenylcyclobutanecarboxylic acid

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Technology Process of 2,2-diphenylcyclobutanecarboxylic acid

There total 8 articles about 2,2-diphenylcyclobutanecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 286850-80-4
2,2-diphenyl-cyclobutanecarboxylic acid methyl ester

: 286850-82-6
2,2-diphenylcyclobutanecarboxylic acid

Guidance literature:: With sodium hydroxide; In water;
DOI:10.1021/jo000095n

Reference yield:

: 5-diazo-2,2-diphenyl-cyclopentanone

: 286850-82-6
2,2-diphenylcyclobutanecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 54 percent / 4 h / Irradiation

2: 52 percent / NaOH / H₂O

With sodium hydroxide; In water; 1: Rearrangement / 2: Hydrolysis;
DOI:10.1021/jo000095n

Reference yield:

: 286850-76-8
2-oxo-3,3-diphenyl-cyclopentanecarbaldehyde

: 286850-82-6
2,2-diphenylcyclobutanecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: p-tosyl azide; triethylamine / CH₂Cl₂ / 17 h / cooling

2: 54 percent / 4 h / Irradiation

3: 52 percent / NaOH / H₂O

With sodium hydroxide; 4-toluenesulfonyl azide; triethylamine; In dichloromethane; water; 1: Diazotization / 2: Rearrangement / 3: Hydrolysis;
DOI:10.1021/jo000095n