N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide

Base Information

Chemical Name:N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide
CAS No.:1015445-15-4
Molecular Formula:C₁₄H₁₉NO₃S
Molecular Weight:281.376
Hs Code.:

Synonyms:N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide

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Technology Process of N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide

There total 1 articles about N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1015445-14-3
4-methyl-N-(2-methyl-2,3-butadienyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzenesulfonylamide

: 1015445-15-4
N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol702966j

Reference yield: 64.0%

: 1015445-15-4
N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide

: 1015445-10-9
4-methyl-N-(2-methyl-2,3-butadienyl)-N-(2-oxoethyl)benzenesulfonamide

Guidance literature:: N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.5h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol702966j