4-methyl-N-(2-methyl-2,3-butadienyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzenesulfonylamide

Base Information

Chemical Name:4-methyl-N-(2-methyl-2,3-butadienyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzenesulfonylamide
CAS No.:1015445-14-3
Molecular Formula:C₂₀H₃₃NO₃SSi
Molecular Weight:395.638
Hs Code.:

Synonyms:4-methyl-N-(2-methyl-2,3-butadienyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzenesulfonylamide

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Chemical Property of 4-methyl-N-(2-methyl-2,3-butadienyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzenesulfonylamide

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Technology Process of 4-methyl-N-(2-methyl-2,3-butadienyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzenesulfonylamide

There total 1 articles about 4-methyl-N-(2-methyl-2,3-butadienyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzenesulfonylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1015445-13-2
4-methyl-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-N-[4-(methanesulfonyloxy)-2-butynyl]benzenesulfonamide

: 917-54-4
methyllithium

: 1015445-14-3
4-methyl-N-(2-methyl-2,3-butadienyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzenesulfonylamide

Guidance literature:: methyllithium; With copper(l) cyanide; lithium chloride; In tetrahydrofuran; diethyl ether; at 0 ℃; for 0.166667h; Inert atmosphere;

4-methyl-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]-N-[4-(methanesulfonyloxy)-2-butynyl]benzenesulfonamide; In tetrahydrofuran; diethyl ether; at 0 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol702966j

Reference yield: 99.0%

: 1015445-14-3
4-methyl-N-(2-methyl-2,3-butadienyl)-N-[2-[[(1,1-dimethylethyl)dimethylsilyl]oxy]ethyl]benzenesulfonylamide

: 1015445-15-4
N-(2-hydroxyethyl)-4-methyl-N-(2-methyl-2,3-butadienyl)benzenesulfonylamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol702966j