tert-Butyldimethylsilyl-2-azido-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

Base Information

Chemical Name:tert-Butyldimethylsilyl-2-azido-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid
CAS No.:120312-04-1
Molecular Formula:C₂₃H₃₇N₃O₇Si
Molecular Weight:495.648
Hs Code.:

Synonyms:tert-Butyldimethylsilyl-2-azido-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tert-Butyldimethylsilyl-2-azido-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

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Technology Process of tert-Butyldimethylsilyl-2-azido-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

There total 2 articles about tert-Butyldimethylsilyl-2-azido-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: 120312-01-8
O-(4-Allyl-2-azido-3,6-di-O-benzyl-2-desoxy-α-D-glucopyranosyl)trichloracetimidat

: 120312-04-1
tert-Butyldimethylsilyl-2-azido-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

Guidance literature:: With trifluorormethanesulfonic acid; In benzene; at 0 ℃; for 12h;

Reference yield:

: 17674-16-7
benzyl triflate

: 106567-62-8
tert-Butyldimethylsilyl-2-azido-6-O-(tert-butyldimethylsilyl)-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

: 120312-04-1
tert-Butyldimethylsilyl-2-azido-6-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

: 120312-05-2
tert-Butyldimethylsilyl-2-azido-4,6-di-O-benzyl-2-desoxy-3-O-<(R)-1-(methoxycarbonyl)ethyl>-β-D-glucopyranosid

Guidance literature:: With pyridine; 2,6-di-tert-butyl-pyridine; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂CL₂, -65 deg C, 20 h; 2.) H₂O, 20 deg C;