methyl 3-((3-chloro-5-fluorophenyl)(2-(methoxycarbonylamino)ethoxy)methyl)-benzoate

Base Information

Chemical Name:methyl 3-((3-chloro-5-fluorophenyl)(2-(methoxycarbonylamino)ethoxy)methyl)-benzoate
CAS No.:1093865-61-2
Molecular Formula:C₁₉H₁₉ClFNO₅
Molecular Weight:395.815
Hs Code.:

Synonyms:methyl 3-((3-chloro-5-fluorophenyl)(2-(methoxycarbonylamino)ethoxy)methyl)-benzoate

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Chemical Property of methyl 3-((3-chloro-5-fluorophenyl)(2-(methoxycarbonylamino)ethoxy)methyl)-benzoate

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Technology Process of methyl 3-((3-chloro-5-fluorophenyl)(2-(methoxycarbonylamino)ethoxy)methyl)-benzoate

There total 7 articles about methyl 3-((3-chloro-5-fluorophenyl)(2-(methoxycarbonylamino)ethoxy)methyl)-benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 1093865-60-1
methyl 3-((2-aminoethoxy)(3-chloro-5-fluorophenyl)methyl)benzoate

: 79-22-1
methyl chloroformate

: 1093865-61-2
methyl 3-((3-chloro-5-fluorophenyl)(2-(methoxycarbonylamino)ethoxy)methyl)-benzoate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 0 - 20 ℃; for 0.5h;

Reference yield:

: 1093865-59-8
C₁₇H₁₃ClFNO₃

: 1093865-61-2
methyl 3-((3-chloro-5-fluorophenyl)(2-(methoxycarbonylamino)ethoxy)methyl)-benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: borane-THF / tetrahydrofuran / 4 h / 60 °C

2: triethylamine / tetrahydrofuran / 0.5 h / 0 - 20 °C

With borane-THF; triethylamine; In tetrahydrofuran;

Reference yield:

: 28987-79-3
m-tolylmagnesium bromide

: 1093865-61-2
methyl 3-((3-chloro-5-fluorophenyl)(2-(methoxycarbonylamino)ethoxy)methyl)-benzoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrahydrofuran / 4 h / -78 - 20 °C

2.1: sodium hydride / acetonitrile / 1 h / 0 °C

2.2: 4 h / -20 - 20 °C

3.1: borane-THF / tetrahydrofuran / 4 h / 60 °C

4.1: triethylamine / tetrahydrofuran / 0.5 h / 0 - 20 °C

With borane-THF; sodium hydride; triethylamine; In tetrahydrofuran; acetonitrile;