2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)-N-[1(E)-dimethylaminoethylidene]benzamide

Base Information

Chemical Name:2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)-N-[1(E)-dimethylaminoethylidene]benzamide
CAS No.:1310532-14-9
Molecular Formula:C₂₂H₂₅BrN₄O
Molecular Weight:441.371
Hs Code.:

Synonyms:2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)-N-[1(E)-dimethylaminoethylidene]benzamide

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Chemical Property of 2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)-N-[1(E)-dimethylaminoethylidene]benzamide

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Technology Process of 2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)-N-[1(E)-dimethylaminoethylidene]benzamide

There total 5 articles about 2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)-N-[1(E)-dimethylaminoethylidene]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 18871-66-4
N,N-dimethylacetamide dimethyl acetal

: 1310532-11-6
2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)benzamide

: 1310532-14-9
2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)-N-[1(E)-dimethylaminoethylidene]benzamide

Guidance literature:: at 110 ℃; for 5h;

Reference yield:

: 364-73-8
4-Bromo-1-fluoro-2-nitrobenzene

: 1310532-14-9
2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)-N-[1(E)-dimethylaminoethylidene]benzamide

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 16 h / 60 °C

2: zinc; ammonium formate / water; methanol / 2 h / 70 °C

3: Oxone / N,N-dimethyl-formamide; water / 2 h / 20 °C

4: ammonium hydroxide; dihydrogen peroxide / water; methanol / 3 h / 20 °C

5: 5 h / 110 °C

With Oxone; ammonium hydroxide; dihydrogen peroxide; ammonium formate; zinc; In tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;

Reference yield:

: 1135351-95-9
4-bromo-N-(tert-butyl)-2-nitroaniline

: 1310532-14-9
2-(5-bromo-1-tert-butyl-1H-benzimidazol-2-yl)-N-[1(E)-dimethylaminoethylidene]benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: zinc; ammonium formate / water; methanol / 2 h / 70 °C

2: Oxone / N,N-dimethyl-formamide; water / 2 h / 20 °C

3: ammonium hydroxide; dihydrogen peroxide / water; methanol / 3 h / 20 °C

4: 5 h / 110 °C

With Oxone; ammonium hydroxide; dihydrogen peroxide; ammonium formate; zinc; In methanol; water; N,N-dimethyl-formamide;