N-(2-(methylcarbamoyl)-4-chloro-6-methylphenyl)-3-(azidomethyl)-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

Base Information

Chemical Name:N-(2-(methylcarbamoyl)-4-chloro-6-methylphenyl)-3-(azidomethyl)-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide
CAS No.:1257070-25-9
Molecular Formula:C₁₉H₁₆Cl₂N₈O₂
Molecular Weight:459.294
Hs Code.:

Synonyms:N-(2-(methylcarbamoyl)-4-chloro-6-methylphenyl)-3-(azidomethyl)-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

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Chemical Property of N-(2-(methylcarbamoyl)-4-chloro-6-methylphenyl)-3-(azidomethyl)-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

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Technology Process of N-(2-(methylcarbamoyl)-4-chloro-6-methylphenyl)-3-(azidomethyl)-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

There total 10 articles about N-(2-(methylcarbamoyl)-4-chloro-6-methylphenyl)-3-(azidomethyl)-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1257070-03-3
C₂₀H₁₉Cl₂N₅O₅S

: 1257070-25-9
N-(2-(methylcarbamoyl)-4-chloro-6-methylphenyl)-3-(azidomethyl)-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

Guidance literature:: With sodium azide; In water; acetone; at 20 ℃; for 20h;
DOI:10.1021/jf102842r

Reference yield:

: 2-amino-5-chloro-3-methylbenzoyl chloride

: 1257070-25-9
N-(2-(methylcarbamoyl)-4-chloro-6-methylphenyl)-3-(azidomethyl)-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

Guidance literature:: Multi-step reaction with 5 steps

1: dichloromethane

2: pyridine / 1 h / 20 °C

3: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

4: organic base / dichloromethane / 0 - 20 °C

5: sodium azide / water; acetone / 20 h / 20 °C

With pyridine; lithium aluminium tetrahydride; sodium azide; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/jf102842r

Reference yield:

: C₁₂H₉Cl₂N₃O₃

: 1257070-25-9
N-(2-(methylcarbamoyl)-4-chloro-6-methylphenyl)-3-(azidomethyl)-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 1 h / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

3: organic base / dichloromethane / 0 - 20 °C

4: sodium azide / water; acetone / 20 h / 20 °C

With pyridine; lithium aluminium tetrahydride; sodium azide; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/jf102842r