dibutyl(2-hydroxybenzyl)phosphine oxide

Base Information

Chemical Name:dibutyl(2-hydroxybenzyl)phosphine oxide
CAS No.:352641-27-1
Molecular Formula:C₁₅H₂₅O₂P
Molecular Weight:268.336
Hs Code.:

Synonyms:dibutyl(2-hydroxybenzyl)phosphine oxide

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Chemical Property of dibutyl(2-hydroxybenzyl)phosphine oxide

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Technology Process of dibutyl(2-hydroxybenzyl)phosphine oxide

There total 2 articles about dibutyl(2-hydroxybenzyl)phosphine oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 109-65-9
1-bromo-butane

: 14707-41-6
2-ethoxy-2,3-dihydro-[d][1,2]oxaphosphole 2-oxide

: 352641-27-1
dibutyl(2-hydroxybenzyl)phosphine oxide

Guidance literature:: 1-bromo-butane; With magnesium; In tetrahydrofuran;

2-ethoxy-2,3-dihydro-[d][1,2]oxaphosphole 2-oxide; In tetrahydrofuran; for 2h; Reflux; Inert atmosphere;

With sulfuric acid; In tetrahydrofuran; water;
DOI:10.1134/S1070363216030063

Reference yield:

: 90-01-7
salicylic alcohol

: 352641-27-1
dibutyl(2-hydroxybenzyl)phosphine oxide

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene / 12 h / Reflux

2.1: magnesium / tetrahydrofuran

2.2: 2 h / Reflux; Inert atmosphere

With magnesium; In tetrahydrofuran; toluene;
DOI:10.1134/S1070363216030063