4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol

Base Information

Chemical Name:4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol
CAS No.:849631-23-8
Molecular Formula:C₁₉H₂₄N₄O₇
Molecular Weight:420.422
Hs Code.:

Synonyms:4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol

Suppliers and Price of 4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol

There total 5 articles about 4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 94-09-7
p-aminoethylbenzoate

: 849631-21-6
4,6-di-O-acetyl-2,5-anhydro-3-azido-3-deoxy-aldehydo-D-altrose

: 849631-24-9
4,6-di-O-acetyl-2,5-anhydro-3-azido-3-deoxy-D-altritol

: 849631-23-8
4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol

Guidance literature:: With sodium tris(acetoxy)borohydride; In 1,2-dichloro-ethane; at 25 ℃; for 18h;
DOI:10.1055/s-2005-922762

Reference yield:

: 849631-19-2
2,5-anhydro-3-azido-3-deoxy-aldehydo-D-altrose dimethylacetal

: 849631-23-8
4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 0 °C

2: aq. TFA / 1 h / 20 °C

3: 47 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 18 h / 25 °C

With pyridine; sodium tris(acetoxy)borohydride; trifluoroacetic acid; In 1,2-dichloro-ethane;
DOI:10.1055/s-2005-922762

Reference yield:

: 849631-20-5
4,6-di-O-acetyl-2,5-anhydro-3-azido-3-deoxy-D-altrose dimethyl acetal

: 849631-23-8
4,6-di-O-acetyl-2,5-anhydro-3-azido-1,3-dideoxy-1-(4-ethoxycarbonyl-phenylamino)-D-altritol

Guidance literature:: Multi-step reaction with 2 steps

1: aq. TFA / 1 h / 20 °C

2: 47 percent / NaBH(OAc)3 / 1,2-dichloro-ethane / 18 h / 25 °C

With sodium tris(acetoxy)borohydride; trifluoroacetic acid; In 1,2-dichloro-ethane;
DOI:10.1055/s-2005-922762