methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate

Base Information

Chemical Name:methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate
CAS No.:452068-51-8
Molecular Formula:C₅₄H₅₄FNO₈
Molecular Weight:864.023
Hs Code.:

methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate

Synonyms:methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate

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Chemical Property of methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate

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Technology Process of methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate

There total 1 articles about methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.8%

: 452068-50-7
(4S)-4-[([4-{(2S,5S,3R,4R,6R)-6-[(benzyloxy)methyl]-3,4,5-tribenzyloxy}perhydro-2H-pyran-2-yl]methyl)phenyl]-1-(4-fluorophenyl)azetidine-2-one

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 452068-51-8
methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate

Guidance literature:: (4S)-4-[([4-{(2S,5S,3R,4R,6R)-6-[(benzyloxy)methyl]-3,4,5-tribenzyloxy}perhydro-2H-pyran-2-yl]methyl)phenyl]-1-(4-fluorophenyl)azetidine-2-one; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 1h;

acrylic acid methyl ester; In tetrahydrofuran; for 0.5h;

With ammonium chloride; In tetrahydrofuran; water;

Reference yield:

: 452068-51-8
methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate

: C₅₃H₅₂FNO₈

Guidance literature:: methyl 3-{[{(4S,3R)-4-[4-{(2S,5S,3R,4R,6R)-6-(benzyloxymethyl)-3,4,5-tribenzyloxy} perhydro-2H-pyran-2-yl]methyl}phenyl]-1-(4-fluorophenyl)oxoazetidine-3-yl}propionate; With methanol; lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 4h;

With hydrogenchloride; In tetrahydrofuran; water;