Au₂(1,4-bis(diphenylphosphino)benzene)(C*C-(4-MeO-Ph))2

Base Information

Chemical Name:Au₂(1,4-bis(diphenylphosphino)benzene)(C*C-(4-MeO-Ph))2
CAS No.:174646-21-0
Molecular Formula:C₄₈H₃₈Au₂O₂P₂
Molecular Weight:1102.71
Hs Code.:

Au<sub>2</sub>(1,4-bis(diphenylphosphino)benzene)(C*C-(4-MeO-Ph))2

Synonyms:Au₂(1,4-bis(diphenylphosphino)benzene)(C*C-(4-MeO-Ph))2

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Chemical Property of Au₂(1,4-bis(diphenylphosphino)benzene)(C*C-(4-MeO-Ph))2

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Technology Process of Au₂(1,4-bis(diphenylphosphino)benzene)(C*C-(4-MeO-Ph))2

There total 1 articles about Au₂(1,4-bis(diphenylphosphino)benzene)(C*C-(4-MeO-Ph))2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 174646-23-2
[Au(C*C-(4-MeO-Ph))]n

: 1179-06-2
1,4-Bis(diphenylphosphino)benzene

: 174646-21-0
Au₂(1,4-bis(diphenylphosphino)benzene)(C*C-(4-MeO-Ph))2

Guidance literature:: In dichloromethane; to suspn. Au complex in CH2Cl2 phosphine was added, mixt. was stirred for 30 min; toluene was added to mixt., passed through alumina, concd., ppt. was centrifugated, washed with PhMe, Et2O, dried in vac.; elem. anal.;
DOI:10.1021/ic801987t

Reference yield: 86.0%

: 64443-05-6
tetrakis(actonitrile)copper(I) hexafluorophosphate

: 174646-21-0
Au₂(1,4-bis(diphenylphosphino)benzene)(C*C-(4-MeO-Ph))2

: [(Au₃Cu₂(C₂C₆H₄OMe)6)Au₃(1,4-bis-(diphenylphosphino)benzene)3][PF₆]2

Guidance literature:: In diethyl ether; dichloromethane; to suspn. Au complex in CH2Cl2-Et2O soln. Cu(NCMe)4PF6 in CH2Cl2 was added dropwise, mixt. was stirred for 30 min; mixt. was evapd., dissolved in acetone, filtered, hexane (or Et2O) was added, ppt. was recrystd. by gas-phase diffusion pentane or Et2O into acetone soln. at 5°C; elem. anal.;
DOI:10.1021/ic801987t