C₄₇H₅₉F₃O₇

Base Information

Chemical Name:C₄₇H₅₉F₃O₇
CAS No.:1268373-62-1
Molecular Formula:C₄₇H₅₉F₃O₇
Molecular Weight:792.976
Hs Code.:

C<sub>47</sub>H<sub>59</sub>F<sub>3</sub>O<sub>7</sub>

Synonyms:C₄₇H₅₉F₃O₇

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₇H₅₉F₃O₇

Chemical Property:

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Technology Process of C₄₇H₅₉F₃O₇

There total 5 articles about C₄₇H₅₉F₃O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1268373-54-1
C₅₃H₆₆F₃NO₉

: 1268373-62-1
C₄₇H₅₉F₃O₇

Guidance literature:: C₅₃H₆₆F₃NO₉; With methanol; lithium borohydride; In tetrahydrofuran; diethyl ether; at 0 ℃; for 0.5h; Inert atmosphere;

With water; ammonium chloride; In tetrahydrofuran; diethyl ether; Saturated solution;
DOI:10.1002/anie.201006230

Reference yield:

: C₁₈H₃₃NO₃Si

: 1268373-62-1
C₄₇H₅₉F₃O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: titanium tetrachloride / dichloromethane / -78 - -40 °C / Inert atmosphere

1.2: 20 °C / Saturated solution

2.1: 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine / dichloromethane / 0.5 h / -60 °C / Inert atmosphere; Molecular sieve

2.2: 21 h / -60 °C / Inert atmosphere

3.1: methanol; lithium borohydride / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C / Inert atmosphere

3.2: Saturated solution

With methanol; lithium borohydride; 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; titanium tetrachloride; 2,4,6-tri-tert-butylpyrimidine; In tetrahydrofuran; diethyl ether; dichloromethane; 1.1: Mukaiyama reaction;
DOI:10.1002/anie.201006230

Reference yield:

: 1268373-46-1
C₁₁H₂₂O

: 1268373-62-1
C₄₇H₅₉F₃O₇

Guidance literature:: Multi-step reaction with 3 steps

1.1: titanium tetrachloride / dichloromethane / -78 - -40 °C / Inert atmosphere

1.2: 20 °C / Saturated solution

2.1: 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; 2,4,6-tri-tert-butylpyrimidine / dichloromethane / 0.5 h / -60 °C / Inert atmosphere; Molecular sieve

2.2: 21 h / -60 °C / Inert atmosphere

3.1: methanol; lithium borohydride / tetrahydrofuran; diethyl ether / 0.5 h / 0 °C / Inert atmosphere

3.2: Saturated solution

With methanol; lithium borohydride; 1-benzenesulfinyl piperidine; trifluoromethylsulfonic anhydride; titanium tetrachloride; 2,4,6-tri-tert-butylpyrimidine; In tetrahydrofuran; diethyl ether; dichloromethane; 1.1: Mukaiyama reaction;
DOI:10.1002/anie.201006230