dibenzyl 2-[1',2'-bis(benzyloxycarbonyl)hydrazinyl]-2-(2'',3''-butadienyl)malonate

Base Information

Chemical Name:dibenzyl 2-[1',2'-bis(benzyloxycarbonyl)hydrazinyl]-2-(2'',3''-butadienyl)malonate
CAS No.:1095073-63-4
Molecular Formula:C₃₇H₃₄N₂O₈
Molecular Weight:634.686
Hs Code.:

Synonyms:dibenzyl 2-[1',2'-bis(benzyloxycarbonyl)hydrazinyl]-2-(2'',3''-butadienyl)malonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl 2-[1',2'-bis(benzyloxycarbonyl)hydrazinyl]-2-(2'',3''-butadienyl)malonate

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Technology Process of dibenzyl 2-[1',2'-bis(benzyloxycarbonyl)hydrazinyl]-2-(2'',3''-butadienyl)malonate

There total 1 articles about dibenzyl 2-[1',2'-bis(benzyloxycarbonyl)hydrazinyl]-2-(2'',3''-butadienyl)malonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1144108-64-4
dibenzyl 2-(2',3'-butadienyl)malonate

: 2449-05-0
dibenzyl azodicarboxylate

: 1095073-63-4
dibenzyl 2-[1',2'-bis(benzyloxycarbonyl)hydrazinyl]-2-(2'',3''-butadienyl)malonate

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2008.09.049

Reference yield:

: 1095073-63-4
dibenzyl 2-[1',2'-bis(benzyloxycarbonyl)hydrazinyl]-2-(2'',3''-butadienyl)malonate

: 589-87-7
1,4-bromoiodobenzene

: 1095074-07-9
1,2,3,3-tetrakis(benzyloxycarbonyl)-5-(R)-(1'-(4-bromophenyl)ethenyl)pyrazolidine

: 1095073-93-0
1,2,3,3-tetrakis(benzyloxycarbonyl)-5-(1'-(4''-bromophenyl)ethenyl)pyrazolidine

Guidance literature:: With silver orthophosphate; (4R,4’R)-2,2’-(propane-2,2-diyl)bis(4-benzyl-4,5-dihydrooxazole); bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; at 20 - 70 ℃; optical yield given as %ee;
DOI:10.1016/j.tet.2008.09.049

Reference yield:

: 3437-95-4,149762-92-5
2-Iodothiophene

: 1095073-63-4
dibenzyl 2-[1',2'-bis(benzyloxycarbonyl)hydrazinyl]-2-(2'',3''-butadienyl)malonate

: 1,2,3,3-tetrakis(benzyloxycarbonyl)-5-(1'-(2''-thienyl)ethenyl)pyrazolidine

: 1095074-05-7
1,2,3,3-tetrakis(benzyloxycarbonyl)-5-(1'-(2''-thienyl)ethenyl)pyrazolidine

Guidance literature:: With silver orthophosphate; (4R,4’R)-2,2’-(propane-2,2-diyl)bis(4-benzyl-4,5-dihydrooxazole); bis(dibenzylideneacetone)-palladium⁽⁰⁾; In tetrahydrofuran; at 20 - 70 ℃; optical yield given as %ee;
DOI:10.1016/j.tet.2008.09.049