{[p-methoxybenzyl-({bis-[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methylbutyl]amine

Base Information

• Chemical Name: {[p-methoxybenzyl-({bis-[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methylbutyl]amine
• CAS No.: 775354-90-0
• Molecular Formula: C₇₀H₈₅N₇O₉
• Molecular Weight: 1168.49

Synonyms:{[p-methoxybenzyl-({bis-[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methylbutyl]amine

Chemical Property of {[p-methoxybenzyl-({bis-[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methylbutyl]amine

Chemical Property:

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Technology Process of {[p-methoxybenzyl-({bis-[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methylbutyl]amine

There total 1 articles about {[p-methoxybenzyl-({bis-[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methylbutyl]amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

N1-(4-amino-3-methyl-butyl)-N1-p-methoxybenzyl-3-methyl-butan-1,4-diamine + 2-(2-methyl-allyl)-isoindole-1,3-dione (6335-03-1) + carbon monoxide (201230-82-2) → {[p-methoxybenzyl-({bis-[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methylbutyl]amine (775354-90-0)

Guidance literature:

With hydrogen; chloro(1,5-cyclooctadiene)rhodium(I) dimer; In toluene; at 130 ℃; for 72h; under 75006 Torr;

DOI:10.1016/j.tet.2004.06.129

Reference yield: 81.0%

{[p-methoxybenzyl-({bis-[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methylbutyl]amine (775354-90-0) → N1-(4-amino-3-methyl-butyl)-N1-{4-[{4-[bis(4-amino-3-methyl-butyl)amino]-3-methyl-butyl}-(4-methoxy-benzyl)amino]-2-methyl-butyl}-3-methyl-butane-1,4-diamine

Guidance literature:

With hydrazine hydrate; In ethanol; dichloromethane; at 50 ℃; for 48h;

DOI:10.1016/j.tet.2004.06.129

Reference yield: 63.0%

{[p-methoxybenzyl-({bis-[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methylbutyl]amine (775354-90-0) → {[p-hydroxybenzyl-({bis[4-(N-phthalimidyl)-3-methyl-butyl]amino}methyl-butyl)amino]methyl-butyl}-bis[4-(N-phthalimidyl)-3-methyl-butyl]amine

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃; for 24h;

DOI:10.1016/j.tet.2004.06.129

upstream raw materials:

2-(2-methyl-allyl)-isoindole-1,3-dione

carbon monoxide

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