4-deoxy-1,2-O-(1-methylethylidene)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol

Base Information

Chemical Name:4-deoxy-1,2-O-(1-methylethylidene)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol
CAS No.:582322-12-1
Molecular Formula:C₂₈H₃₇NO₇
Molecular Weight:499.604
Hs Code.:

Synonyms:4-deoxy-1,2-O-(1-methylethylidene)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol

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Chemical Property of 4-deoxy-1,2-O-(1-methylethylidene)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol

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Technology Process of 4-deoxy-1,2-O-(1-methylethylidene)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol

There total 3 articles about 4-deoxy-1,2-O-(1-methylethylidene)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 24424-99-5
di-tert-butyl dicarbonate

: (3aR,4R,5R,6S,7R,7aS)-5-Amino-6,7-bis-benzyloxy-2,2-dimethyl-hexahydro-benzo[1,3]dioxol-4-ol

: 582322-13-2
4-deoxy-1,2-O-(1-methylethylidene)-4-(carboxyamino)-5,6-bis-O-(phenylmethyl)-D-myo-inositol intramol. 3,4-ester

: 582322-12-1
4-deoxy-1,2-O-(1-methylethylidene)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol

Guidance literature:: With dmap; In acetonitrile; at 20 ℃; for 20h;
DOI:10.1248/cpb.51.100

Reference yield:

: 582322-02-9
4-deoxy-1,2-O-(1-methylethylidene)-4-[(phenylmethoxy)amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol

: 582322-12-1
4-deoxy-1,2-O-(1-methylethylidene)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: LiAlH₄ / tetrahydrofuran / 1 h / Heating

2: 48 percent / DMAP / acetonitrile / 20 h / 20 °C

With dmap; lithium aluminium tetrahydride; In tetrahydrofuran; acetonitrile;
DOI:10.1248/cpb.51.100

Reference yield:

: 4,5-O-(1-methylethylidene)-2,3-bis-O-(phenylmethyl)-D-gluco-hexodialdose 1-[O-(phenylmethyl)oxime]

: 582322-12-1
4-deoxy-1,2-O-(1-methylethylidene)-4-[[(1,1-dimethylethoxy)carbonyl]amino]-5,6-bis-O-(phenylmethyl)-D-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: 59 percent / Bu₃SnH; AIBN / benzene / 1.5 h / Heating

2: LiAlH₄ / tetrahydrofuran / 1 h / Heating

3: 48 percent / DMAP / acetonitrile / 20 h / 20 °C

With dmap; lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In tetrahydrofuran; acetonitrile; benzene;
DOI:10.1248/cpb.51.100