(S)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester

Base Information

Chemical Name:(S)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester
CAS No.:865367-01-7
Molecular Formula:C₁₈H₁₇ClO₄
Molecular Weight:332.784
Hs Code.:

Synonyms:(S)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester

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Chemical Property of (S)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester

Chemical Property:

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Technology Process of (S)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester

There total 3 articles about (S)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 53911-68-5
3-(4-chlorophenyl)glutaric anhydride

: 100-51-6,185532-71-2
benzyl alcohol

: (R)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester

: 865367-01-7
(S)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester

Guidance literature:: With Novozym 435; In di-isopropyl ether; at 20 ℃; for 792h; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2005.06.025

Reference yield:

: 35271-74-0
3-(4-chlorophenyl)pentane-1,5-dioic acid

: 865367-01-7
(S)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: AcCl / 3 h

2: Novozym 435 / diisopropyl ether / 792 h / 20 °C

With Novozym 435; acetyl chloride; In di-isopropyl ether;
DOI:10.1016/j.tetasy.2005.06.025

Reference yield:

: 104-88-1
4-chlorobenzaldehyde

: 865367-01-7
(S)-3-(4-chloro-phenyl)pentanedioic acid monobenzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1.1: piperidine / 72 h / 20 °C

1.2: aq. KOH / 3 h / 80 - 95 °C

2.1: AcCl / 3 h

3.1: Novozym 435 / diisopropyl ether / 792 h / 20 °C

With piperidine; Novozym 435; acetyl chloride; In di-isopropyl ether;
DOI:10.1016/j.tetasy.2005.06.025