(1-allyl-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexa-2,4-dien-1-yl)methyl pivalate

Base Information

Chemical Name:(1-allyl-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexa-2,4-dien-1-yl)methyl pivalate
CAS No.:1172604-33-9
Molecular Formula:C₂₁H₃₆O₃Si
Molecular Weight:364.601
Hs Code.:

Synonyms:(1-allyl-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexa-2,4-dien-1-yl)methyl pivalate

Suppliers and Price of (1-allyl-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexa-2,4-dien-1-yl)methyl pivalate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1-allyl-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexa-2,4-dien-1-yl)methyl pivalate

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Technology Process of (1-allyl-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexa-2,4-dien-1-yl)methyl pivalate

There total 1 articles about (1-allyl-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexa-2,4-dien-1-yl)methyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1172604-32-8
(1-allyl-4-oxocyclohex-2-en-1-yl)methyl pivalate

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1172604-33-9
(1-allyl-4-{[tert-butyl(dimethyl)silyl]oxy}cyclohexa-2,4-dien-1-yl)methyl pivalate

Guidance literature:: (1-allyl-4-oxocyclohex-2-en-1-yl)methyl pivalate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -90 - -80 ℃; for 1.5h; Inert atmosphere;

tert-butyldimethylsilyl chloride; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; hexane; at -80 - 20 ℃; Inert atmosphere;
DOI:10.1002/anie.200900447