thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Base Information

Chemical Name:thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside
CAS No.:866890-13-3
Molecular Formula:C₄₈H₅₅N₃O₁₂Si
Molecular Weight:894.063
Hs Code.:

Synonyms:thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Suppliers and Price of thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

There total 6 articles about thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 212246-68-9
thexyldimethylsilyl 2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

: 671194-42-6
2,3-di-O-benzoyl-4,6-O-benzylidene-1-O-trichloroacetimidoyl α-D-galactopyranose

: 866890-13-3
thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1080/07328300500176312

Reference yield:

: 866890-12-2
1,2,3-tri-O-benzoyl-4,6-O-benzylidene-D-galactopyranose

: 866890-13-3
thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 29 percent / hydrazinium acetate / dimethylformamide / 3 h / 45 °C

2: 89 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 0.75 h / 20 °C

3: 83 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 1 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; hydrazinium monoacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/07328300500176312

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 866890-13-3
thexyldimethylsilyl (2,3-di-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranosyl)-(1->3)-2-azido-4,6-O-benzylidene-2-deoxy-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / 4-methylbenzenesulfonic acid / dimethylformamide / 5 h / 50 °C

2: 83 percent / trimethylsilyl trifluoromethanesulfonate / CH₂Cl₂ / 1 h / 20 °C

With trimethylsilyl trifluoromethanesulfonate; toluene-4-sulfonic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1080/07328300500176312