3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O-(2-phthalimidoethyl)-N⁴-benzoylcytidine

Base Information

• Chemical Name: 3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O-(2-phthalimidoethyl)-N⁴-benzoylcytidine
• CAS No.: 1037523-06-0
• Molecular Formula: C₃₈H₅₀N₄O₉Si₂
• Molecular Weight: 763.007

Synonyms:3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O-(2-phthalimidoethyl)-N⁴-benzoylcytidine

Chemical Property of 3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O-(2-phthalimidoethyl)-N⁴-benzoylcytidine

Chemical Property:

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Technology Process of 3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O-(2-phthalimidoethyl)-N⁴-benzoylcytidine

There total 1 articles about 3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O-(2-phthalimidoethyl)-N⁴-benzoylcytidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

2-(1,3-dioxoisoindolin-2-yl)ethyl trifluoromethanesulfonate (127175-39-7) + 1-[3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl]-N4-benzoylcytosine (69304-43-4) → 3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O-(2-phthalimidoethyl)-N4-benzoylcytidine (1037523-06-0) + 3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O,N3-bis(2-phthalimidoethyl)-N4-benzoylcytidine + 3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O,N4-bis(2-phthalimidoethyl)-N4-benzoylcytidine (1037523-16-2)

Guidance literature:

With sodium hydride; In dichloromethane; at -40 - 0 ℃;

DOI:10.1021/jo800451m

Reference yield: 82.0%

3',5'-O-(tetraisopropyldisiloxane-1,3-diyl)-2'-O-(2-phthalimidoethyl)-N4-benzoylcytidine (1037523-06-0) → 2'-O-(2-phthalimidoethyl)-N4-benzoylcytidine (1037523-26-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 1h;

DOI:10.1021/jo800451m

upstream raw materials:

2-(1,3-dioxoisoindolin-2-yl)ethyl trifluoromethanesulfonate

1-[3,5-O-(1,1,3,3-tetraisopropyldisiloxane-1,3-diyl)-β-D-ribofuranosyl]-N⁴-benzoylcytosine

Downstream raw materials:

2'-O-(2-phthalimidoethyl)-N⁴-benzoylcytidine

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