C₂₆H₃₁N₃O₃

Base Information

Chemical Name:C₂₆H₃₁N₃O₃
CAS No.:1613625-05-0
Molecular Formula:C₂₆H₃₁N₃O₃
Molecular Weight:433.55
Hs Code.:

C<sub>26</sub>H<sub>31</sub>N<sub>3</sub>O<sub>3</sub>

Synonyms:C₂₆H₃₁N₃O₃

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Chemical Property of C₂₆H₃₁N₃O₃

Chemical Property:

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Technology Process of C₂₆H₃₁N₃O₃

There total 15 articles about C₂₆H₃₁N₃O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1613625-04-9
C₃₁H₃₉N₃O₅

: 1613625-05-0
C₂₆H₃₁N₃O₃

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; 1,4-dioxane; at 20 ℃; for 6h;

Reference yield:

: 10465-20-0
γ-(4-methoxy-1-naphthyl)butyric acid

: 1613625-05-0
C₂₆H₃₁N₃O₃

Guidance literature:: Multi-step reaction with 15 steps

1.1: n-butyllithium / tetrahydrofuran / 0.75 h / -78 °C

1.2: 3.5 h / 0 - 20 °C

2.1: potassium hexamethylsilazane / tetrahydrofuran / 0.5 h / -78 °C

2.2: -78 °C

2.3: 16 h / -78 - 27 °C

3.1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 °C

4.1: hydrogen; palladium 10% on activated carbon / water / 3 h / 20 °C / 760.05 Torr

5.1: acetic acid; hydrogen bromide / 4 h / Reflux

6.1: acetyl chloride / 4 h / 0 °C / Reflux

7.1: sodium hydrogencarbonate / methanol; water / 3 h / 0 - 20 °C

8.1: pyridine / 2.5 h / 0 - 20 °C

9.1: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / acetonitrile; hexane / 5 h / Inert atmosphere; Reflux

10.1: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C

11.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / 0 °C

12.1: ammonia / methanol / 18 h / 0 - 20 °C

13.1: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

14.1: triethylamine / dichloromethane / 2 h / 0 - 20 °C

15.1: hydrogenchloride / tetrahydrofuran; 1,4-dioxane / 6 h / 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; tri-tert-butyl phosphine; palladium 10% on activated carbon; ammonia; water; hydrogen bromide; hydrogen; dihydrogen peroxide; potassium hexamethylsilazane; sodium hydrogencarbonate; acetic acid; triethylamine; acetyl chloride; sodium hydroxide; lithium hydroxide; isobutyl chloroformate; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; dichloromethane; water; acetonitrile;

Reference yield:

: 1613624-92-2
(S)-3-((S)-2-azido-4-(4-methoxynaphthalen-1-yl)butanoyl)-4-benzyloxazolidin-2-one

: 1613625-05-0
C₂₆H₃₁N₃O₃

Guidance literature:: Multi-step reaction with 13 steps

1: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water / 3 h / 0 °C

2: hydrogen; palladium 10% on activated carbon / water / 3 h / 20 °C / 760.05 Torr

3: acetic acid; hydrogen bromide / 4 h / Reflux

4: acetyl chloride / 4 h / 0 °C / Reflux

5: sodium hydrogencarbonate / methanol; water / 3 h / 0 - 20 °C

6: pyridine / 2.5 h / 0 - 20 °C

7: tri-tert-butyl phosphine; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine / acetonitrile; hexane / 5 h / Inert atmosphere; Reflux

8: sodium hydroxide; water / tetrahydrofuran; methanol / 3 h / 20 °C

9: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / 0 °C

10: ammonia / methanol / 18 h / 0 - 20 °C

11: hydrogen; palladium 10% on activated carbon / ethanol / 16 h / 20 °C / 760.05 Torr

12: triethylamine / dichloromethane / 2 h / 0 - 20 °C

13: hydrogenchloride / tetrahydrofuran; 1,4-dioxane / 6 h / 20 °C

With 4-methyl-morpholine; pyridine; hydrogenchloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; tri-tert-butyl phosphine; palladium 10% on activated carbon; ammonia; water; hydrogen bromide; hydrogen; dihydrogen peroxide; sodium hydrogencarbonate; acetic acid; triethylamine; acetyl chloride; sodium hydroxide; lithium hydroxide; isobutyl chloroformate; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; dichloromethane; water; acetonitrile;