N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester

Base Information

Chemical Name:N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester
CAS No.:130327-97-8
Molecular Formula:C₂₆H₄₃N₃O₈
Molecular Weight:525.643
Hs Code.:

N-(1,1-dimethylethoxycarbonyl)-N-<2-<N-(1,1-dimethylethoxycarbonyl)-N-(2-cyclohexylethyl)amino>ethyl>glycine N-succinimide ester

Synonyms:N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester

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Chemical Property of N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester

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Technology Process of N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester

There total 5 articles about N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 6066-82-6
1-hydroxy-pyrrolidine-2,5-dione

: 130327-96-7
N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine

: 130327-97-8
N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester

Guidance literature:: With N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; In dichloromethane; for 20h; Ambient temperature;
DOI:10.1021/jm00171a038

Reference yield:

: 10258-93-2
N-(2-cyclohexyl-ethyl)-ethylenediamine

: 130327-97-8
N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester

Guidance literature:: Multi-step reaction with 3 steps

1: 11.1 g / H₂ / 5percent Pd/C / ethanol; H₂O / 2016.9 Torr / Ambient temperature

2: NaOH / H₂O; tetrahydrofuran / Ambient temperature

3: 59 percent / 1-cyclohexyl-3-(2-morpholinoethyl)carbodiimide metho-p-toluenesulfonate / CH₂Cl₂ / 20 h / Ambient temperature

With sodium hydroxide; hydrogen; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm00171a038

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 130327-97-8
N-(1,1-dimethylethoxycarbonyl)-N-<2-ethyl>glycine N-succinimide ester

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / H₂O; tetrahydrofuran / Ambient temperature

2: 59 percent / 1-cyclohexyl-3-(2-morpholinoethyl)carbodiimide metho-p-toluenesulfonate / CH₂Cl₂ / 20 h / Ambient temperature

With sodium hydroxide; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; In tetrahydrofuran; dichloromethane; water;
DOI:10.1021/jm00171a038