Technology Process of C58H82N2O17Si
There total 7 articles about C58H82N2O17Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
methanol;
at 20 ℃;
for 11h;
DOI:10.1016/j.tet.2005.05.087
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: t-BuOK; DMPU / tetrahydrofuran / 0.25 h / -70 °C
1.2: 55 percent / tetrahydrofuran / 3 h / -70 °C
2.1: 55 percent / NaN3; CAN / acetonitrile / 0 °C
3.1: 76 percent / NaBH4 / tetrahydrofuran; ethanol / 96 h / -30 °C
4.1: 80 percent / DCC; DMAP; PTSA / toluene / 1 h / 70 °C
5.1: 90 percent / H2 / Pd/C / methanol / 11 h / 20 °C
With
dmap; 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; sodium tetrahydroborate; sodium azide; ammonium cerium(IV) nitrate; potassium tert-butylate; hydrogen; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; toluene; acetonitrile;
DOI:10.1016/j.tet.2005.05.087
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 76 percent / NaBH4 / tetrahydrofuran; ethanol / 96 h / -30 °C
2: 80 percent / DCC; DMAP; PTSA / toluene / 1 h / 70 °C
3: 90 percent / H2 / Pd/C / methanol / 11 h / 20 °C
With
dmap; sodium tetrahydroborate; hydrogen; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; toluene;
DOI:10.1016/j.tet.2005.05.087
