2-hydroxymethyl-14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6,9,12-tetraoxatetradecanol

Base Information

Chemical Name:2-hydroxymethyl-14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6,9,12-tetraoxatetradecanol
CAS No.:145839-46-9
Molecular Formula:C₄₈H₅₈O₁₁
Molecular Weight:810.982
Hs Code.:

Synonyms:2-hydroxymethyl-14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6,9,12-tetraoxatetradecanol

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Chemical Property of 2-hydroxymethyl-14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6,9,12-tetraoxatetradecanol

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Technology Process of 2-hydroxymethyl-14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6,9,12-tetraoxatetradecanol

There total 10 articles about 2-hydroxymethyl-14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6,9,12-tetraoxatetradecanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 145839-45-8
2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane

: 145839-46-9
2-hydroxymethyl-14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6,9,12-tetraoxatetradecanol

Guidance literature:: With sulfuric acid; In ethanol; for 2h; Heating;
DOI:10.1002/chem.19970030719

Reference yield:

: 978-86-9
4-tritylphenol

: 145839-46-9
2-hydroxymethyl-14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6,9,12-tetraoxatetradecanol

Guidance literature:: Multi-step reaction with 4 steps

1: K₂CO₃ / dimethylformamide / 96 h / 70 °C

2: TBAF / tetrahydrofuran / 3 h / 70 °C

3: 97 percent / NaH / tetrahydrofuran / Heating

4: 71 percent / conc. H₂SO₄ / ethanol / 2 h / Heating

With sulfuric acid; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;
DOI:10.1002/chem.19970030719

Reference yield:

: 134881-72-4
1,4-bis-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)benzene

: 145839-46-9
2-hydroxymethyl-14-[4-(2-{2-[2-(4-tritylphenoxy)ethoxy]ethoxy}ethoxy)phenoxy]-3,6,9,12-tetraoxatetradecanol

Guidance literature:: Multi-step reaction with 6 steps

1: 38 percent / imidazole / dimethylformamide / 3 h / Ambient temperature

2: 84 percent / Et₃N, DMAP / CH₂Cl₂ / 15 h / 4 °C

3: K₂CO₃ / dimethylformamide / 96 h / 70 °C

4: TBAF / tetrahydrofuran / 3 h / 70 °C

5: 97 percent / NaH / tetrahydrofuran / Heating

6: 71 percent / conc. H₂SO₄ / ethanol / 2 h / Heating

With 1H-imidazole; dmap; sulfuric acid; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.19970030719