2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane

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Chemical Name:2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane
CAS No.:145839-45-8
Molecular Formula:C₅₅H₆₂O₁₁
Molecular Weight:899.091
Hs Code.:

Synonyms:2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane

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Chemical Property of 2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane

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Technology Process of 2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane

There total 9 articles about 2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 145839-44-7
Toluene-4-sulfonic acid 2-(2-phenyl-[1,3]dioxan-5-yloxy)-ethyl ester

: 145839-41-4
2-<2-<2-<4-<2-<2-<2-(4-triphenylmethylphenoxy)ethoxy>ethoxy>ethoxy>phenoxy>ethoxy>ethoxy>ethanol

: 145839-45-8
2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane

Guidance literature:: With sodium hydride; In tetrahydrofuran; Heating;
DOI:10.1002/chem.19970030719

Reference yield:

: 978-86-9
4-tritylphenol

: 145839-45-8
2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane

Guidance literature:: Multi-step reaction with 3 steps

1: K₂CO₃ / dimethylformamide / 96 h / 70 °C

2: TBAF / tetrahydrofuran / 3 h / 70 °C

3: 97 percent / NaH / tetrahydrofuran / Heating

With tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1002/chem.19970030719

Reference yield:

: 134881-72-4
1,4-bis-(2-(2-(2-hydroxyethoxy)ethoxy)ethoxy)benzene

: 145839-45-8
2-Phenyl-5-{2-[2-(2-{2-[4-(2-{2-[2-(4-trityl-phenoxy)-ethoxy]-ethoxy}-ethoxy)-phenoxy]-ethoxy}-ethoxy)-ethoxy]-ethoxy}-[1,3]dioxane

Guidance literature:: Multi-step reaction with 5 steps

1: 38 percent / imidazole / dimethylformamide / 3 h / Ambient temperature

2: 84 percent / Et₃N, DMAP / CH₂Cl₂ / 15 h / 4 °C

3: K₂CO₃ / dimethylformamide / 96 h / 70 °C

4: TBAF / tetrahydrofuran / 3 h / 70 °C

5: 97 percent / NaH / tetrahydrofuran / Heating

With 1H-imidazole; dmap; tetrabutyl ammonium fluoride; sodium hydride; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.19970030719