3,5-dimethoxy-4-acetoxybenzoic acid 4-(N,N′-tert-butylcarbonylguanidino)butyl ester

Base Information

Chemical Name:3,5-dimethoxy-4-acetoxybenzoic acid 4-(N,N′-tert-butylcarbonylguanidino)butyl ester
CAS No.:1260119-23-0
Molecular Formula:C₂₆H₃₉N₃O₁₀
Molecular Weight:553.61
Hs Code.:

Synonyms:3,5-dimethoxy-4-acetoxybenzoic acid 4-(N,N′-tert-butylcarbonylguanidino)butyl ester

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Chemical Property of 3,5-dimethoxy-4-acetoxybenzoic acid 4-(N,N′-tert-butylcarbonylguanidino)butyl ester

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Technology Process of 3,5-dimethoxy-4-acetoxybenzoic acid 4-(N,N′-tert-butylcarbonylguanidino)butyl ester

There total 4 articles about 3,5-dimethoxy-4-acetoxybenzoic acid 4-(N,N′-tert-butylcarbonylguanidino)butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 6318-20-3
O-acetylsyringic acid

: 208465-10-5
N²,N³-bis(tert-butoxycarbonyl)-N¹-(4-hydroxybutyl)guanidine

: 1260119-23-0
3,5-dimethoxy-4-acetoxybenzoic acid 4-(N,N′-tert-butylcarbonylguanidino)butyl ester

Guidance literature:: With dmap; diisopropyl-carbodiimide; In dichloromethane; at 20 ℃;

Reference yield:

: 530-57-4
3,5-dimethoxy-4-hydroxybenzoic acid

: 1260119-23-0
3,5-dimethoxy-4-acetoxybenzoic acid 4-(N,N′-tert-butylcarbonylguanidino)butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / 20 °C

2: 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide / dichloromethane / 5 h / 20 °C

With triethylamine; 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.ejmech.2011.05.073

Reference yield:

: 322474-21-5
N,N'-bis-Boc-S-methyl-isothiourea

: 1260119-23-0
3,5-dimethoxy-4-acetoxybenzoic acid 4-(N,N′-tert-butylcarbonylguanidino)butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: N,N-dimethyl-formamide / 3.5 h / 20 °C

2: 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide / dichloromethane / 5 h / 20 °C

With 4-(dimethylamino)pyridinium tosylate; diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.05.073