(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2PCH₂CH₂P(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2

Base Information

• Chemical Name: (C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2PCH₂CH₂P(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2
• CAS No.: 1038436-27-9
• Molecular Formula: C₇₈H₁₀₈N₄O₄P₂Si₄
• Molecular Weight: 1340.03

Synonyms:(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2PCH₂CH₂P(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2

Chemical Property of (C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2PCH₂CH₂P(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2

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Technology Process of (C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2PCH₂CH₂P(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2

There total 1 articles about (C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2PCH₂CH₂P(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

Br(C6H4-4-CH2CH2SiMe2CH2OC6H4-3-NMe2) (1038436-20-2) + 1,2-bis(dichlorophosphino)ethane (28240-69-9) → (C6H4-4-CH2CH2SiMe2CH2OC6H4-3-NMe2)2PCH2CH2P(C6H4-4-CH2CH2SiMe2CH2OC6H4-3-NMe2)2 (1038436-27-9)

Guidance literature:

Br(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂); With tert.-butyl lithium; In tetrahydrofuran; pentane; at -78 ℃; for 1h;

1,2-bis(dichlorophosphino)ethane; In tetrahydrofuran; pentane; at -78 - 20 ℃; Further stages.;

DOI:10.1016/j.jorganchem.2008.03.015

Reference yield:

dichloro(1,5-cyclooctadiene)palladium(II) (12107-56-1) + (C6H4-4-CH2CH2SiMe2CH2OC6H4-3-NMe2)2PCH2CH2P(C6H4-4-CH2CH2SiMe2CH2OC6H4-3-NMe2)2 (1038436-27-9) → [PdCl2((C6H4-4-CH2CH2SiMe2CH2OC6H4-3-NMe2)2PCH2CH2P(C6H4-4-CH2CH2SiMe2CH2OC6H4-3-NMe2)2)]

Guidance literature:

In tetrahydrofuran; (Ar); using Schlenk techniques; treatment of PdCl2(COD) with (CH2P(C6H4C2H4SiMe2CH2OC6H4NMe2)2)2 in THF; removal of volatiles; monitoring by NMR;

DOI:10.1016/j.jorganchem.2008.03.015

upstream raw materials:

Br(C₆H₄-4-CH₂CH₂SiMe₂CH₂OC₆H₄-3-NMe₂)

1,2-bis(dichlorophosphino)ethane

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