Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆

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Chemical Name:Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆
CAS No.:84190-22-7
Molecular Formula:C₇₆H₆₉P₆Pt₂*F₆P
Molecular Weight:1703.35
Hs Code.:

Pt<sub>2</sub>(CH<sub>3</sub>)((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3<sup>(1+)</sup>*PF<sub>6</sub><sup>(1-)</sup>=(Pt<sub>2</sub>(CH<sub>3</sub>)((C<sub>6</sub>H<sub>5</sub>)2PCH<sub>2</sub>P(C<sub>6</sub>H<sub>5</sub>)2)3)PF<sub>6</sub>

Synonyms:Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆

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Chemical Property of Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆

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Technology Process of Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆

There total 2 articles about Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 17084-13-8
potassium hexafluorophosphate

: 84190-20-5
methyl-(η1-dppm)-bis(μ-dppm)-diplatinum iodide

: 84190-22-7
Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆

Guidance literature:: In dichloromethane; water; a soln. of KPF6 in water was added to a CH2Cl2 soln. of Pt-complex, mixt. was stirred for 45 min; org. phase was sepd., washed with water, dried (molecular sieve), cyclohexane was added slowly, crystals were recovered by filtration and driedin vacuo; elem. anal. for the adduct with 0.35 CH2Cl2;
DOI:10.1021/om00083a009

Reference yield: 67.0%

: 17084-13-8
potassium hexafluorophosphate

: 14221-02-4
tetrakis(triphenylphosphine)platinum

: 2071-20-7
bis-diphenylphosphinomethane

: 84190-22-7
Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆

Guidance literature:: With methyl iodide; In benzene; Pt(PPh3)4 and dppm were dissolved in benzene under N2, resulting soln. was stirred with MeI at room temp. for 3.5 h, filtered, ppt. washed withbenzene and cyclohexane, dried, dissolved in CH2Cl2, aq. soln. of KPF6 was added, mixt. stirred for 45 min; org. phase was sepd., washed with water, dried (molecular sieve), cyclohexane was added slowly, crystals were recovered by filtration and driedin vacuo;
DOI:10.1021/om00083a009

Reference yield: 57.0%

: 84190-22-7
Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)((C₆H₅)2PCH₂P(C₆H₅)2)3)PF₆

: 89378-04-1
Pt₂(CH₃)2I((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*PF₆^(1-)=(Pt₂(CH₃)2I((C₆H₅)2PCH₂P(C₆H₅)2)2)PF₆

Guidance literature:: With methyl iodide; In dichloromethane; MeI was added under N2 to a soln. of Pt-complex in CH2Cl2, mixt. was stirred for 20 h at 20°C; solvent was evapd. in a stream of N2 to the point of crystn., cyclohexane was added, ppt. filtered, recrystd. from CH2Cl2 and cyclohexane; elem. anal.;
DOI:10.1021/om00083a009