ortho-(R)-N,N-dimethyl-<(dimethyl)-(1-methylethenyl)-silyl>-phenylethylamine

Base Information

Chemical Name:ortho-(R)-N,N-dimethyl-<(dimethyl)-(1-methylethenyl)-silyl>-phenylethylamine
CAS No.:230949-42-5
Molecular Formula:C₁₅H₂₅NSi
Molecular Weight:247.456
Hs Code.:

Synonyms:ortho-(R)-N,N-dimethyl-<(dimethyl)-(1-methylethenyl)-silyl>-phenylethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ortho-(R)-N,N-dimethyl-<(dimethyl)-(1-methylethenyl)-silyl>-phenylethylamine

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Technology Process of ortho-(R)-N,N-dimethyl-<(dimethyl)-(1-methylethenyl)-silyl>-phenylethylamine

There total 2 articles about ortho-(R)-N,N-dimethyl-<(dimethyl)-(1-methylethenyl)-silyl>-phenylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 13291-18-4
isopropenylmagnesium bromide

: 230949-41-4
ortho-(R)-N,N-dimethyl-<(dimethyl)-methoxy-silyl>phenylethylamine

: 230949-42-5
ortho-(R)-N,N-dimethyl-<(dimethyl)-(1-methylethenyl)-silyl>-phenylethylamine

Guidance literature:: In tetrahydrofuran;
DOI:10.1016/S0040-4020(99)00350-6

Reference yield:

: 19342-01-9
(S)-N,N-dimethyl-1-phenylethylamine

: 230949-42-5
ortho-(R)-N,N-dimethyl-<(dimethyl)-(1-methylethenyl)-silyl>-phenylethylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 30 percent / n-BuLi, TMEDA / diethyl ether; hexane / 120 h

2: 67 percent / tetrahydrofuran

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1016/S0040-4020(99)00350-6