adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane

Base Information

Chemical Name:adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane
CAS No.:1335151-14-8
Molecular Formula:C₂₄H₃₀O₆
Molecular Weight:414.499
Hs Code.:

Synonyms:adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane

Suppliers and Price of adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane

There total 2 articles about adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 700-58-3
2-Adamantanone

: 1335151-12-6
methyl 4-(4,4-dihydroperoxycyclohexyl)benzoate

: 1335151-14-8
adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane

Guidance literature:: With rhenium(VII) oxide; In dichloromethane; at 20 ℃; for 12h;
DOI:10.1016/j.bmcl.2011.07.024

Reference yield:

: 137464-98-3
4-(4-oxocyclohexyl)benzoic acid methyl ester

: 1335151-14-8
adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; iodine / acetonitrile / 24 h / 20 °C

2: rhenium(VII) oxide / dichloromethane / 12 h / 20 °C

With dihydrogen peroxide; iodine; rhenium(VII) oxide; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.07.024

Reference yield: 99.0%

: 1335151-14-8
adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane

: 1335151-22-8
adamantane-2-spiro-3'-9'-(4'-carboxyphenyl)-1',2',4',5'-tetraoxaspiro[5.5]undecane

Guidance literature:: adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane; With water; potassium hydroxide; In tetrahydrofuran; ethanol; at 50 ℃; for 20h;

With acetic acid; In water;
DOI:10.1016/j.bmcl.2011.07.024