adamantane-2-spiro-3'-9'-(4'-carboxyphenyl)-1',2',4',5'-tetraoxaspiro[5.5]undecane

Base Information

Chemical Name:adamantane-2-spiro-3'-9'-(4'-carboxyphenyl)-1',2',4',5'-tetraoxaspiro[5.5]undecane
CAS No.:1335151-22-8
Molecular Formula:C₂₃H₂₈O₆
Molecular Weight:400.472
Hs Code.:

Synonyms:adamantane-2-spiro-3'-9'-(4'-carboxyphenyl)-1',2',4',5'-tetraoxaspiro[5.5]undecane

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Chemical Property of adamantane-2-spiro-3'-9'-(4'-carboxyphenyl)-1',2',4',5'-tetraoxaspiro[5.5]undecane

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Technology Process of adamantane-2-spiro-3'-9'-(4'-carboxyphenyl)-1',2',4',5'-tetraoxaspiro[5.5]undecane

There total 2 articles about adamantane-2-spiro-3'-9'-(4'-carboxyphenyl)-1',2',4',5'-tetraoxaspiro[5.5]undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1335151-14-8
adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane

: 1335151-22-8
adamantane-2-spiro-3'-9'-(4'-carboxyphenyl)-1',2',4',5'-tetraoxaspiro[5.5]undecane

Guidance literature:: adamantane-2-spiro-3'-9'-[4'-(methoxycarbonyl)phenyl]-1',2',4',5'-tetraoxaspiro[5.5]undecane; With water; potassium hydroxide; In tetrahydrofuran; ethanol; at 50 ℃; for 20h;

With acetic acid; In water;
DOI:10.1016/j.bmcl.2011.07.024

Reference yield:

: 137464-98-3
4-(4-oxocyclohexyl)benzoic acid methyl ester

: 1335151-22-8
adamantane-2-spiro-3'-9'-(4'-carboxyphenyl)-1',2',4',5'-tetraoxaspiro[5.5]undecane

Guidance literature:: Multi-step reaction with 3 steps

1: dihydrogen peroxide; iodine / acetonitrile / 24 h / 20 °C

2: rhenium(VII) oxide / dichloromethane / 12 h / 20 °C

3: water; potassium hydroxide / tetrahydrofuran; ethanol / 20 h / 50 °C

With water; dihydrogen peroxide; iodine; rhenium(VII) oxide; potassium hydroxide; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2011.07.024