Technology Process of C32H36N2O6
There total 4 articles about C32H36N2O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
2-(3,4-bis((4-methoxybenzyl)oxy)phenyl)-2-oxoacetic acid;
With
1-chloro-1-(dimethylamino)-2-methyl-1-propene;
In
tetrahydrofuran;
at 0 ℃;
for 1h;
4-aminomethylquinuclidine;
In
tetrahydrofuran;
at 0 - 20 ℃;
for 1h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium iodide; potassium carbonate / N,N-dimethyl acetamide / 1.5 h / 50 °C
2.1: pyridine; selenium(IV) oxide / 24 h / 80 °C
3.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / tetrahydrofuran / 1 h / 0 °C
3.2: 1 h / 0 - 20 °C
With
pyridine; selenium(IV) oxide; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; potassium carbonate; sodium iodide;
In
tetrahydrofuran; N,N-dimethyl acetamide;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: pyridine; selenium(IV) oxide / 24 h / 80 °C
2.1: 1-chloro-1-(dimethylamino)-2-methyl-1-propene / tetrahydrofuran / 1 h / 0 °C
2.2: 1 h / 0 - 20 °C
With
pyridine; selenium(IV) oxide; 1-chloro-1-(dimethylamino)-2-methyl-1-propene;
In
tetrahydrofuran;