(Z)-1-[1-(3,4-dichlorophenyl)cyclobutyl]-N-hydroxy-1-(pyridin-2-yl)methanimine

Base Information

Chemical Name:(Z)-1-[1-(3,4-dichlorophenyl)cyclobutyl]-N-hydroxy-1-(pyridin-2-yl)methanimine
CAS No.:1358804-04-2
Molecular Formula:C₁₆H₁₄Cl₂N₂O
Molecular Weight:321.206
Hs Code.:

Synonyms:(Z)-1-[1-(3,4-dichlorophenyl)cyclobutyl]-N-hydroxy-1-(pyridin-2-yl)methanimine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-1-[1-(3,4-dichlorophenyl)cyclobutyl]-N-hydroxy-1-(pyridin-2-yl)methanimine

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Technology Process of (Z)-1-[1-(3,4-dichlorophenyl)cyclobutyl]-N-hydroxy-1-(pyridin-2-yl)methanimine

There total 2 articles about (Z)-1-[1-(3,4-dichlorophenyl)cyclobutyl]-N-hydroxy-1-(pyridin-2-yl)methanimine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.2%

: 1358804-41-7
[1-(3,4-dichlorophenyl)cyclobutyl](pyridin-2-yl)methanone

: 1358804-04-2
(Z)-1-[1-(3,4-dichlorophenyl)cyclobutyl]-N-hydroxy-1-(pyridin-2-yl)methanimine

: 1432493-02-1
(E)-[1-(3,4-dichlorophenyl)cyclobutyl](pyridin-2-yl)methanone oxime

Guidance literature:: With pyridine; hydroxylamine hydrochloride; at 20 ℃; for 48h;

Reference yield:

: 109-04-6
2-bromo-pyridine

: 84467-19-6
1-(3,4-dichlorophenyl)-1-cyclobutanecarbonitrile

: 1358804-04-2
(Z)-1-[1-(3,4-dichlorophenyl)cyclobutyl]-N-hydroxy-1-(pyridin-2-yl)methanimine

: 1432493-02-1
(E)-[1-(3,4-dichlorophenyl)cyclobutyl](pyridin-2-yl)methanone oxime

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -75 °C

1.2: 0.5 h / 50 - 60 °C

2.1: pyridine; hydroxylamine hydrochloride / 48 h / 20 °C

With pyridine; n-butyllithium; hydroxylamine hydrochloride; In tetrahydrofuran; hexane;