2,6-bis(4-dibutylaminostyryl)-9,10-distyrylanthracene

Base Information

Chemical Name:2,6-bis(4-dibutylaminostyryl)-9,10-distyrylanthracene
CAS No.:1493783-46-2
Molecular Formula:C₆₂H₆₈N₂
Molecular Weight:841.235
Hs Code.:

Synonyms:2,6-bis(4-dibutylaminostyryl)-9,10-distyrylanthracene

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Chemical Property of 2,6-bis(4-dibutylaminostyryl)-9,10-distyrylanthracene

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Technology Process of 2,6-bis(4-dibutylaminostyryl)-9,10-distyrylanthracene

There total 4 articles about 2,6-bis(4-dibutylaminostyryl)-9,10-distyrylanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1430076-58-6
2,6-bis(diethylphosphorylmethyl)-9,10-distyrylanthracene

: 90134-10-4
4-(N,N-dibutylamino)benzaldehyde

: 1493783-46-2
2,6-bis(4-dibutylaminostyryl)-9,10-distyrylanthracene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.dyepig.2013.09.037

Reference yield:

: 62-53-3
aniline

: 1493783-46-2
2,6-bis(4-dibutylaminostyryl)-9,10-distyrylanthracene

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / N,N-dimethyl-formamide / 24 h / 80 °C

2: trichlorophosphate / 6 h / 20 °C

3: potassium tert-butylate / tetrahydrofuran / 20 °C / Inert atmosphere

With potassium tert-butylate; potassium carbonate; trichlorophosphate; In tetrahydrofuran; N,N-dimethyl-formamide; 3: |Wittig-Horner Reaction;
DOI:10.1039/c3tc32035a

Reference yield:

: 333426-62-3
2,6-bis(diethoxyphosphorylmethyl)-9,10-dibromoanthracene

: 1493783-46-2
2,6-bis(4-dibutylaminostyryl)-9,10-distyrylanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; tris-(o-tolyl)phosphine; triethylamine / tetrahydrofuran / 24 h / 80 °C / Sealed tube; Inert atmosphere

2: potassium tert-butylate / tetrahydrofuran / 20 °C / Inert atmosphere

With potassium tert-butylate; palladium diacetate; triethylamine; tris-(o-tolyl)phosphine; In tetrahydrofuran; 1: |Heck Reaction / 2: |Wittig-Horner Reaction;
DOI:10.1039/c3tc32035a