4-(DIBUTYLAMINO)BENZALDEHYDE 98

Base Information

• Chemical Name: 4-(DIBUTYLAMINO)BENZALDEHYDE 98
• CAS No.: 90134-10-4
• Molecular Formula: C15H23 N O
• Molecular Weight: 233.354
• Hs Code.: 2922399090
• Mol file: 90134-10-4.mol

Synonyms:4-(Dibutylamino)benzaldehyde;4-(N,N-Dibutylamino)benzaldehyde; N,N-Dibutyl-4-aminobenzaldehyde;p-(Dibutylamino)benzaldehyde; p-(N,N-Dibutylamino)benzaldehyde

Chemical Property of 4-(DIBUTYLAMINO)BENZALDEHYDE 98

Chemical Property:

• Vapor Pressure: 3.49E-06mmHg at 25°C
• Refractive Index: n20/D 1.587(lit.)
• Boiling Point: 198-200℃/3mmHg(lit.)
• PKA: 2.95±0.32(Predicted)
• Flash Point: 113°C
• PSA: 20.31000
• Density: 0.978g/mLat 25℃(lit.)
• LogP: 3.90570

Purity/Quality:

95% ^*data from raw suppliers

4-(Dibutylamino)benzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 26-37/39

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 4-(Dibutylamino)benzaldehyde is a stain/dye. Dyes and metabolites.

Technology Process of 4-(DIBUTYLAMINO)BENZALDEHYDE 98

There total 13 articles about 4-(DIBUTYLAMINO)BENZALDEHYDE 98 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-Dibutylaniline (613-29-6) + N,N-dimethyl-formamide (68-12-2,33513-42-7) → 4-(N,N-dibutylamino)benzaldehyde (90134-10-4)

Guidance literature:

With trichlorophosphate; at 95 ℃; for 7.25h; Cooling with ice; Inert atmosphere;

DOI:10.1021/jo202015m

Reference yield: 85.0%

→ 4-(N,N-dibutylamino)benzaldehyde (90134-10-4)

Guidance literature:

With trichlorophosphate; at -4 - 100 ℃;

Reference yield: 78.0%

4-fluorobenzaldehyde (459-57-4) + dibutylamine (111-92-2) → 4-(N,N-dibutylamino)benzaldehyde (90134-10-4)

Guidance literature:

4-fluorobenzaldehyde; dibutylamine; With potassium carbonate; In dimethyl sulfoxide; for 0.25h; sonication;

In dimethyl sulfoxide; at 100 ℃; for 48h;

DOI:10.1021/ma0305333

upstream raw materials:

formaldehyd

N-Dibutylaniline

hexamethylenetetramine

N,N-dimethyl-formamide

Downstream raw materials:

5-[1-(4-Dibutylamino-phenyl)-meth-(Z)-ylidene]-imidazolidine-2,4-dione

5-[1-(4-Dibutylamino-phenyl)-meth-(Z)-ylidene]-2-thioxo-imidazolidin-4-one

4-{2-[4-(dibutylamino)phenyl]-2-hydroxyethyl}-4'-methyl-2,2'-bipyridine

(E)-4-(dibutylamino)-4'-nitrostilbene