methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate

Base Information

Chemical Name:methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate
CAS No.:1372195-51-1
Molecular Formula:C₂₆H₂₉NO₅S
Molecular Weight:467.586
Hs Code.:

Synonyms:methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate

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Chemical Property of methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate

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Technology Process of methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate

There total 6 articles about methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372195-49-7
methyl 4-(N,N-bis(4-methoxybenzyl)sulfamoyl)-3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)butanoate

: 1372195-51-1
methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 15h;

Reference yield:

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 1372195-51-1
methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene; tetrahydrofuran / 15 h / 20 °C / Cooling with ice

2.1: lithium hexamethyldisilazane / tetrahydrofuran / -20 °C

2.2: -20 °C

2.3: 20 °C

3.1: sodium methylate / tetrahydrofuran; methanol / 1 h

3.2: 17 h / Reflux

4.1: sodium chloride / N,N-dimethyl-formamide / 2.5 h / Reflux

5.1: trifluoroacetic acid / dichloromethane / 15 h / 20 °C

With di-isopropyl azodicarboxylate; sodium methylate; triphenylphosphine; trifluoroacetic acid; sodium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;

Reference yield:

: 1372195-46-4
2-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis(4-methoxybenzyl)ethenesulfonamide

: 1372195-51-1
methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium methylate / tetrahydrofuran; methanol / 1 h

1.2: 17 h / Reflux

2.1: sodium chloride / N,N-dimethyl-formamide / 2.5 h / Reflux

3.1: trifluoroacetic acid / dichloromethane / 15 h / 20 °C

With sodium methylate; trifluoroacetic acid; sodium chloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;