5-[4-[[3-(2,6-dimethylphenyl)phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-on

Base Information

Chemical Name:5-[4-[[3-(2,6-dimethylphenyl)phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-on
CAS No.:1372192-11-4
Molecular Formula:C₂₅H₂₅NO₄S
Molecular Weight:435.544
Hs Code.:

Synonyms:5-[4-[[3-(2,6-dimethylphenyl)phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-on

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Chemical Property of 5-[4-[[3-(2,6-dimethylphenyl)phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-on

Chemical Property:

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Technology Process of 5-[4-[[3-(2,6-dimethylphenyl)phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-on

There total 7 articles about 5-[4-[[3-(2,6-dimethylphenyl)phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1372195-51-1
methyl 3-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-4-sulfamoylbutanoate

: 1372192-11-4
5-[4-[[3-(2,6-dimethylphenyl)phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-on

Guidance literature:: In tetrahydrofuran; methanol; for 1h;

Reference yield:

: 1372195-46-4
2-(4-((2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)-N,N-bis(4-methoxybenzyl)ethenesulfonamide

: 1372192-11-4
5-[4-[[3-(2,6-dimethylphenyl)phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-on

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / tetrahydrofuran; methanol / 1 h

1.2: 17 h / Reflux

2.1: sodium chloride / N,N-dimethyl-formamide / 2.5 h / Reflux

3.1: trifluoroacetic acid / dichloromethane / 15 h / 20 °C

4.1: tetrahydrofuran; methanol / 1 h

With sodium methylate; trifluoroacetic acid; sodium chloride; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 691905-27-8
(2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methanol

: 1372192-11-4
5-[4-[[3-(2,6-dimethylphenyl)phenyl]methoxy]phenyl]-1,1-dioxo-1,2-thiazinan-3-on

Guidance literature:: Multi-step reaction with 6 steps

1.1: triphenylphosphine; di-isopropyl azodicarboxylate / toluene; tetrahydrofuran / 15 h / 20 °C / Cooling with ice

2.1: lithium hexamethyldisilazane / tetrahydrofuran / -20 °C

2.2: -20 °C

2.3: 20 °C

3.1: sodium methylate / tetrahydrofuran; methanol / 1 h

3.2: 17 h / Reflux

4.1: sodium chloride / N,N-dimethyl-formamide / 2.5 h / Reflux

5.1: trifluoroacetic acid / dichloromethane / 15 h / 20 °C

6.1: tetrahydrofuran; methanol / 1 h

With di-isopropyl azodicarboxylate; sodium methylate; triphenylphosphine; trifluoroacetic acid; sodium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;