Technology Process of C25H34N2O5
There total 5 articles about C25H34N2O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C13H17NO6;
With
benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
at 70 ℃;
for 0.166667h;
2,6-diisopropylbenzenamine;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 12h;
DOI:10.1021/ja4025148
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: sodium acetate; acetic acid; zinc / 2 h / 60 - 90 °C
2.1: acetic acid; bromine; sulfuryl dichloride / 5 h / 10 - 20 °C
2.2: 1 h / 20 °C
3.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h
4.1: palladium 10% on activated carbon; formic acid; hydrogen / methanol / 2 h
5.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 70 °C
5.2: 12 h / 20 °C
With
dmap; formic acid; sulfuryl dichloride; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; bromine; sodium acetate; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; zinc;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja4025148
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: palladium 10% on activated carbon; formic acid; hydrogen / methanol / 2 h
2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h / 70 °C
2.2: 12 h / 20 °C
With
formic acid; palladium 10% on activated carbon; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; N-ethyl-N,N-diisopropylamine;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1021/ja4025148
