C₅₃H₆₀N₇O₁₆P

Base Information

Chemical Name:C₅₃H₆₀N₇O₁₆P
CAS No.:833480-34-5
Molecular Formula:C₅₃H₆₀N₇O₁₆P
Molecular Weight:1082.07
Hs Code.:

C<sub>53</sub>H<sub>60</sub>N<sub>7</sub>O<sub>16</sub>P

Synonyms:C₅₃H₆₀N₇O₁₆P

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₃H₆₀N₇O₁₆P

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Technology Process of C₅₃H₆₀N₇O₁₆P

There total 9 articles about C₅₃H₆₀N₇O₁₆P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 833480-32-3
C₅₉H₇₄N₇O₁₆PSi

: 833480-34-5
C₅₃H₆₀N₇O₁₆P

Guidance literature:: With tetrabutyl ammonium fluoride; acetic acid; In tetrahydrofuran; at 0 ℃; for 5h;
DOI:10.1021/jo048253o

Reference yield:

: 833480-25-4
{(2R,3S)-5-Azido-2-[bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-tetrahydro-furan-3-yloxy}-tert-butyl-dimethyl-silane

: 833480-34-5
C₅₃H₆₀N₇O₁₆P

Guidance literature:: Multi-step reaction with 7 steps

1.1: hydrogen / Lindlar's catalyst / ethanol / 1.25 h / 2327.17 Torr

2.1: 43 percent / diisopropylethylamine / ethanol / 14 h / 70 °C

3.1: diisopropylethylamine; PyBOP / CH₂Cl₂ / 0 - 25 °C

4.1: 12 percent / FeCl₃*6H₂O / acetonitrile / 1.5 h / 25 °C

5.1: tetrazole / acetonitrile / 0 - 25 °C

5.2: 47 percent / tert-butyl hydroperoxide / acetonitrile; decane / 0.5 h / 0 °C

6.1: H₂; diisopropylethylamine / Pd/C / tetrahydrofuran / 2 h / 25 °C / 4137.18 Torr

6.2: 6 percent / pyridine / tetrahydrofuran / 0.17 h / 0 °C

7.1: 83 percent / Bu₄NF*3H₂O; acetic acid / tetrahydrofuran / 5 h / 0 °C

With 1H-tetrazole; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; iron(III) chloride; acetic acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; Lindlar's catalyst; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jo048253o

Reference yield:

: 418759-83-8
(4S,5R)-5-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-4-(tert-butyl-dimethyl-silanyloxy)-tetrahydro-furan-2-ylamine

: 833480-34-5
C₅₃H₆₀N₇O₁₆P

Guidance literature:: Multi-step reaction with 6 steps

1.1: 43 percent / diisopropylethylamine / ethanol / 14 h / 70 °C

2.1: diisopropylethylamine; PyBOP / CH₂Cl₂ / 0 - 25 °C

3.1: 12 percent / FeCl₃*6H₂O / acetonitrile / 1.5 h / 25 °C

4.1: tetrazole / acetonitrile / 0 - 25 °C

4.2: 47 percent / tert-butyl hydroperoxide / acetonitrile; decane / 0.5 h / 0 °C

5.1: H₂; diisopropylethylamine / Pd/C / tetrahydrofuran / 2 h / 25 °C / 4137.18 Torr

5.2: 6 percent / pyridine / tetrahydrofuran / 0.17 h / 0 °C

6.1: 83 percent / Bu₄NF*3H₂O; acetic acid / tetrahydrofuran / 5 h / 0 °C

With 1H-tetrazole; tetrabutyl ammonium fluoride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; iron(III) chloride; acetic acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In tetrahydrofuran; ethanol; dichloromethane; acetonitrile;
DOI:10.1021/jo048253o