diethyl {4-[(E)-phenyldiazenyl]benzene-1,3-diyl}biscarbamate

Base Information

Chemical Name:diethyl {4-[(E)-phenyldiazenyl]benzene-1,3-diyl}biscarbamate
CAS No.:75953-40-1
Molecular Formula:C₁₈H₂₀N₄O₄
Molecular Weight:356.381
Hs Code.:
DSSTox Substance ID:DTXSID901040034

Synonyms:DTXSID901040034;STK958551;AKOS003888771;75953-40-1;diethyl {4-[(E)-phenyldiazenyl]benzene-1,3-diyl}biscarbamate;Carbamic acid, [4-(phenylazo)-1,3-phenylene]bis-, diethyl ester (9CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diethyl {4-[(E)-phenyldiazenyl]benzene-1,3-diyl}biscarbamate

Chemical Property:

XLogP3:3.6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:8
Exact Mass:356.14845513
Heavy Atom Count:26
Complexity:480

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCOC(=O)NC1=CC(=C(C=C1)N=NC2=CC=CC=C2)NC(=O)OCC

Technology Process of diethyl {4-[(E)-phenyldiazenyl]benzene-1,3-diyl}biscarbamate

There total 3 articles about diethyl {4-[(E)-phenyldiazenyl]benzene-1,3-diyl}biscarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 541-41-3
chloroformic acid ethyl ester

: 495-54-5
2,4-diaminoazobenzene

: 75953-40-1
2,4-bis(ethoxycarbonylamino)azobenzene

Guidance literature:: With pyridine; 1. 0 deg C, 2 h; 2. room temperature, 20 h;

Reference yield:

: 108-45-2,64554-26-3,76583-20-5
m-phenylenediamine

: 75953-40-1
2,4-bis(ethoxycarbonylamino)azobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1. NaNO₂, 37percent HCl / 1. H₂O, 0 deg C; 2. 0 deg C, 2 h

2: 100 percent / pyridine / 1. 0 deg C, 2 h; 2. room temperature, 20 h

With pyridine; hydrogenchloride; sodium nitrite;

Reference yield:

: 62-53-3
aniline

: 75953-40-1
2,4-bis(ethoxycarbonylamino)azobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 1. NaNO₂, 37percent HCl / 1. H₂O, 0 deg C; 2. 0 deg C, 2 h

2: 100 percent / pyridine / 1. 0 deg C, 2 h; 2. room temperature, 20 h

With pyridine; hydrogenchloride; sodium nitrite;