3-allyloxy-4-chloroanisole

Base Information

• Chemical Name: 3-allyloxy-4-chloroanisole
• CAS No.: 898826-74-9
• Molecular Formula: C₁₀H₁₁ClO₂
• Molecular Weight: 198.649
• Mol file: 898826-74-9.mol

Synonyms:3-allyloxy-4-chloroanisole

Chemical Property of 3-allyloxy-4-chloroanisole

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of 3-allyloxy-4-chloroanisole

There total 1 articles about 3-allyloxy-4-chloroanisole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Chlororesorcinol (95-88-5) → 3-allyloxy-4-chloroanisole (898826-74-9)

Guidance literature:

Multi-step reaction with 2 steps

1: K₂CO₃ / acetone / 3 h / Heating

2: K₂CO₃ / acetone / 6 h / Heating

With potassium carbonate; In acetone;

DOI:10.1002/chem.200501392

Reference yield: 55.0%

3-allyloxy-4-chloroanisole (898826-74-9) → 3-chloromethyl-2,3-dihydro-6-methoxybenzofuran + 6-methoxy-3-methylbenzofuran (29040-52-6)

Guidance literature:

With acetone; benzene; In ethyl acetate; at 20 ℃; for 16h; Further Variations:; Solvents; Reagents; time; Product distribution; UV-irradiation;

DOI:10.1002/chem.200501392

Reference yield:

3-allyloxy-4-chloroanisole (898826-74-9) → 3-chloromethyl-2,3-dihydro-6-methoxybenzofuran + O-methylresorcine (150-19-6) + 6-methoxy-3-methylbenzofuran (29040-52-6)

Guidance literature:

With caesium carbonate; acetone; In acetonitrile; at 20 ℃; for 22h; Further Variations:; Solvents; Reagents; time; Product distribution; UV-irradiation;

DOI:10.1002/chem.200501392

upstream raw materials:

4-Chlororesorcinol

Downstream raw materials:

6-methoxy-3-methylbenzofuran

O-methylresorcine