N-allyl-N-((2-((allyloxy)(phenyl)methyl)phenyl)ethynyl)methanesulfonamide

Base Information

Chemical Name:N-allyl-N-((2-((allyloxy)(phenyl)methyl)phenyl)ethynyl)methanesulfonamide
CAS No.:1638755-31-3
Molecular Formula:C₂₂H₂₃NO₃S
Molecular Weight:381.496
Hs Code.:

Synonyms:N-allyl-N-((2-((allyloxy)(phenyl)methyl)phenyl)ethynyl)methanesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-allyl-N-((2-((allyloxy)(phenyl)methyl)phenyl)ethynyl)methanesulfonamide

Chemical Property:

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Technology Process of N-allyl-N-((2-((allyloxy)(phenyl)methyl)phenyl)ethynyl)methanesulfonamide

There total 6 articles about N-allyl-N-((2-((allyloxy)(phenyl)methyl)phenyl)ethynyl)methanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59639-96-2
N-allylmethanesulfonamide

: 1638755-09-5
1-((allyloxy)(phenyl)methyl)-2-(bromoethynyl)benzene

: 1638755-31-3
N-allyl-N-((2-((allyloxy)(phenyl)methyl)phenyl)ethynyl)methanesulfonamide

Guidance literature:: With 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; potassium carbonate; In toluene; at 65 ℃;
DOI:10.1002/chem.201403040

Reference yield:

: 77123-58-1
2-[2-(trimethylsilyl)ethynyl]benzaldehyde

: 1638755-31-3
N-allyl-N-((2-((allyloxy)(phenyl)methyl)phenyl)ethynyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: magnesium; iodine

1.2: 1 h / -78 - 20 °C

2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.17 h / Cooling with ice

2.2: 2 h / 20 °C

3.1: potassium carbonate; methanol / 1 h / 20 °C

4.1: N-Bromosuccinimide; silver nitrate / acetone / 1 h / 20 °C

5.1: potassium carbonate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate / toluene / 65 °C

With methanol; N-Bromosuccinimide; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; iodine; sodium hydride; potassium carbonate; silver nitrate; magnesium; In tetrahydrofuran; acetone; toluene; mineral oil;
DOI:10.1002/chem.201403040

Reference yield:

: 1610735-40-4
1-((allyloxy)(phenyl)methyl)-2-ethynylbenzene

: 1638755-31-3
N-allyl-N-((2-((allyloxy)(phenyl)methyl)phenyl)ethynyl)methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; silver nitrate / acetone / 1 h / 20 °C

2: potassium carbonate; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate / toluene / 65 °C

With N-Bromosuccinimide; 1,10-Phenanthroline; copper(ll) sulfate pentahydrate; potassium carbonate; silver nitrate; In acetone; toluene;
DOI:10.1002/chem.201403040