phenylalanylvalylphenylalanine amide hydrochloride

Base Information

Chemical Name:phenylalanylvalylphenylalanine amide hydrochloride
CAS No.:96886-63-4
Molecular Formula:C₂₃H₃₀N₄O₃*ClH
Molecular Weight:446.977
Hs Code.:

Synonyms:phenylalanylvalylphenylalanine amide hydrochloride

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Chemical Property of phenylalanylvalylphenylalanine amide hydrochloride

Chemical Property:

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Technology Process of phenylalanylvalylphenylalanine amide hydrochloride

There total 15 articles about phenylalanylvalylphenylalanine amide hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 96886-62-3
N_α-diphenylphosphinoylphenylalanylvalylphenylalanine amide

: 96886-63-4
phenylalanylvalylphenylalanine amide hydrochloride

Guidance literature:: With hydrogenchloride; In methanol; at 0 ℃; for 1.58333h;

Reference yield:

: 1161-13-3
N-Cbz-L-Phe

: 96886-63-4
phenylalanylvalylphenylalanine amide hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1: 83 percent / DCCI, ammonium salt of hydroxybenzotriazole / CH₂Cl₂ / Ambient temperature

2: 96 percent / H₂ / 10percent Pd/C / dimethylformamide / 18 h / Ambient temperature

3: CH₂Cl₂; dimethylformamide / 0.67 h / 0 °C

4: 90 percent / 10M methanolic HCl / methanol; CDCl₃ / 1.67 h / 0 °C

5: N-methylmorpholine / CH₂Cl₂; dimethylformamide / 0.5 h / 0 °C

6: 90 percent / 10M methanolic HCl / methanol / 1.58 h / 0 °C

With 4-methyl-morpholine; hydrogenchloride; ammonium salt of hydroxybenzotriazole; hydrogen; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; chloroform-d1; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 96886-63-4
phenylalanylvalylphenylalanine amide hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1: 75 percent / 4M aq. NaOH, 1M aq. NaHCO₃ / 18 h / Ambient temperature

2: 83 percent / DCCI, ammonium salt of hydroxybenzotriazole / CH₂Cl₂ / Ambient temperature

3: 96 percent / H₂ / 10percent Pd/C / dimethylformamide / 18 h / Ambient temperature

4: CH₂Cl₂; dimethylformamide / 0.67 h / 0 °C

5: 90 percent / 10M methanolic HCl / methanol; CDCl₃ / 1.67 h / 0 °C

6: N-methylmorpholine / CH₂Cl₂; dimethylformamide / 0.5 h / 0 °C

7: 90 percent / 10M methanolic HCl / methanol / 1.58 h / 0 °C

With 4-methyl-morpholine; hydrogenchloride; sodium hydroxide; ammonium salt of hydroxybenzotriazole; hydrogen; sodium hydrogencarbonate; dicyclohexyl-carbodiimide; palladium on activated charcoal; In methanol; chloroform-d1; dichloromethane; N,N-dimethyl-formamide;