C₄₁H₅₃NO₁₃

Base Information

Chemical Name:C₄₁H₅₃NO₁₃
CAS No.:1369430-78-3
Molecular Formula:C₄₁H₅₃NO₁₃
Molecular Weight:767.871
Hs Code.:

C<sub>41</sub>H<sub>53</sub>NO<sub>13</sub>

Synonyms:C₄₁H₅₃NO₁₃

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Chemical Property of C₄₁H₅₃NO₁₃

Chemical Property:

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Technology Process of C₄₁H₅₃NO₁₃

There total 11 articles about C₄₁H₅₃NO₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1240304-75-9
u202fN-(2,2-dimethylbut-3-enoyl)-2-methylalanine

: 1359976-62-7
(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-{5-[(4-bromophenyl)methyl]-2-methoxy-4-(propan-2-yl)phenyl}-D-glucitol

: 1369430-78-3
C₄₁H₅₃NO₁₃

Guidance literature:: With tri-o-tolylphosphine; palladium diacetate; triethylamine; In acetonitrile; at 120 ℃; for 0.5h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 1240304-71-5
(1S)-2,3,4,6-tetra-O-acetyl-1,5-anhydro-1-[5-bromo-2-methoxy-4-(propan-2-yl)phenyl]-D-glucitol

: 1369430-78-3
C₄₁H₅₃NO₁₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium methylate / methanol / 2 h / 20 °C

1.2: 2 h / 20 °C / Cooling with ice

2.1: n-butyllithium / hexane; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

2.2: 0.75 h

2.3: 14 h / 20 °C

3.1: acetic anhydride / pyridine / 5 h / 20 °C / Cooling with ice

3.2: 0.67 h / Inert atmosphere; Cooling with ice

4.1: triethylamine; palladium diacetate; tri-o-tolylphosphine / acetonitrile / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation

With n-butyllithium; tri-o-tolylphosphine; sodium methylate; palladium diacetate; acetic anhydride; triethylamine; In tetrahydrofuran; pyridine; methanol; hexane; acetonitrile;

Reference yield:

: 1240304-64-6
1-iodo-2-methoxy-4-(propan-2-yl)benzene

: 1369430-78-3
C₄₁H₅₃NO₁₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: n-butyllithium / hexane / 0.08 h / -78 °C / Inert atmosphere

1.2: 0.58 h / Cooling with ice

2.1: triethylsilane; boron trifluoride diethyl etherate / acetonitrile; chloroform / 1 h / 4 °C / Inert atmosphere

3.1: bromine / 1 h / 20 °C

4.1: sodium methylate / methanol / 2 h / 20 °C

4.2: 2 h / 20 °C / Cooling with ice

5.1: n-butyllithium / hexane; tetrahydrofuran / 0.17 h / -78 °C / Inert atmosphere

5.2: 0.75 h

5.3: 14 h / 20 °C

6.1: acetic anhydride / pyridine / 5 h / 20 °C / Cooling with ice

6.2: 0.67 h / Inert atmosphere; Cooling with ice

7.1: triethylamine; palladium diacetate; tri-o-tolylphosphine / acetonitrile / 0.5 h / 120 °C / Inert atmosphere; Microwave irradiation

With triethylsilane; n-butyllithium; boron trifluoride diethyl etherate; tri-o-tolylphosphine; bromine; sodium methylate; palladium diacetate; acetic anhydride; triethylamine; In tetrahydrofuran; pyridine; methanol; hexane; chloroform; acetonitrile;