Acetic acid N'-(1-acetyl-2-oxo-propylidene)-N-(4-nitro-phenyl)-hydrazide

Base Information

Chemical Name:Acetic acid N'-(1-acetyl-2-oxo-propylidene)-N-(4-nitro-phenyl)-hydrazide
CAS No.:137156-90-2
Molecular Formula:C₁₃H₁₃N₃O₅
Molecular Weight:291.263
Hs Code.:

Synonyms:Acetic acid N'-(1-acetyl-2-oxo-propylidene)-N-(4-nitro-phenyl)-hydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid N'-(1-acetyl-2-oxo-propylidene)-N-(4-nitro-phenyl)-hydrazide

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Technology Process of Acetic acid N'-(1-acetyl-2-oxo-propylidene)-N-(4-nitro-phenyl)-hydrazide

There total 1 articles about Acetic acid N'-(1-acetyl-2-oxo-propylidene)-N-(4-nitro-phenyl)-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-36-5
acetyl chloride

: 50711-98-3
pentane-2,3,4-trione-3-(4-nitro-phenylhydrazone)

: 137156-90-2
Acetic acid N'-(1-acetyl-2-oxo-propylidene)-N-(4-nitro-phenyl)-hydrazide

Guidance literature:: With sodium hydride; Yield given. Multistep reaction; 1.) THF, from 0 to 10 deg C, 40 min, 2.) THF, from 0 to 5 deg C, 2 min;

Reference yield: 28.0%

: 137156-90-2
Acetic acid N'-(1-acetyl-2-oxo-propylidene)-N-(4-nitro-phenyl)-hydrazide

: 137827-74-8
3-[(4-Nitro-phenyl)-hydrazono]-heptane-2,4,6-trione

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 - 10 ℃; for 2h;

Reference yield:

: 137156-90-2
Acetic acid N'-(1-acetyl-2-oxo-propylidene)-N-(4-nitro-phenyl)-hydrazide

: 137156-95-7
3-acetyl-6-methyl-1-(4-nitrophenyl)-1H-pyridazin-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 28 percent / NaH / tetrahydrofuran / 2 h / 0 - 10 °C

2: AcOH / 2 h / Heating

With sodium hydride; acetic acid; In tetrahydrofuran;